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[ CAS No. 6836-97-1 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 6836-97-1
Chemical Structure| 6836-97-1
Structure of 6836-97-1 * Storage: {[proInfo.prStorage]}
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Product Details of [ 6836-97-1 ]

CAS No. :6836-97-1 MDL No. :MFCD01687225
Formula : C10H11NO Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 161.20 Pubchem ID :-
Synonyms :

Safety of [ 6836-97-1 ]

Signal Word:Warning Class:
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330 UN#:
Hazard Statements:H302-H315-H319 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 6836-97-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6836-97-1 ]

[ 6836-97-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6836-97-1 ]
  • [ 1005-37-4 ]
  • 1-(2-amino-6-methylaminopyrimidin-4-yl)-3-phenylpyrrolidin-2-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
16 mg With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In 1,4-dioxane; at 120℃; for 4h;Inert atmosphere; Sealed tube; 6-Chloro-N4-methyl-2,4-pyrimidinediamine (150 mg; 0,9 mmol) was dissolved in 1 ,4-Dioxane (5 ml) and under nitrogen was added 3-phenyl- pyrrolidin-2-one (168 mg; 1 mmol), 4,5-Bis(diphenylphosphino)-9,9- dimethylxanthene (55 mg; 0,1 mmol), potassium (III) phosphate (402 mg; 1,9 mmol) and Tris-(dibenzylidenaceton)-dipalladium (0) (87 mg; 0,1 mmol). The reaction was stirred for 4 firs at 120C in the microwave. The reactions were filtrated and evaporated to dryness. The residue was purified by prep. HPLC giving 16 mg of the desired product as light brown solid. (0634)
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