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Chemical Structure| 68395-81-3 Chemical Structure| 68395-81-3

Structure of 68395-81-3

Chemical Structure| 68395-81-3

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Product Details of [ 68395-81-3 ]

CAS No. :68395-81-3
Formula : C16H13NO
M.W : 235.28
SMILES Code : C1(CC2=CC=CC=C2)=NC=C(C3=CC=CC=C3)O1

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Application In Synthesis of [ 68395-81-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 68395-81-3 ]

[ 68395-81-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1006-68-4 ]
  • [ 100-44-7 ]
  • [ 68395-81-3 ]
YieldReaction ConditionsOperation in experiment
83% With NHC-Pd(II)-Im; lithium tert-butoxide; In toluene; at 130℃; for 3h;Inert atmosphere; Sealed tube; Under N2 atmosphere, LiOtBu (1.0 mmol), benzoxazole 2a (0.6 mmol), NHC-Pd(II)-Im complex 1 (2.0 mol %), dry toluene (2.0 mL) and benzyl chloride 3a (0.5 mmol) were successively added into a sealed tube. The mixture was stirred vigorously at 130 C for 3 h. After cooling to room temperature, the reaction mixture was concentrated under reduced pressure and the residue was purified by flash column chromatography on silica gel to afford pure product 4a.
 

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