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Chemical Structure| 6848-73-3 Chemical Structure| 6848-73-3

Structure of 6848-73-3

Chemical Structure| 6848-73-3

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Product Details of [ 6848-73-3 ]

CAS No. :6848-73-3
Formula : C10H14O3
M.W : 182.22
SMILES Code : OC(C)C1=C(C(OC)=CC=C1)OC
MDL No. :MFCD11499064

Safety of [ 6848-73-3 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 6848-73-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6848-73-3 ]

[ 6848-73-3 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 6848-73-3 ]
  • [ 38480-94-3 ]
YieldReaction ConditionsOperation in experiment
65% With potassium dichromate; sulfuric acid; In water; 18F 2',3'-Dimethoxyacetophenone A solution of potassium dichromate (24.76 g), water (124 ml) and concentrated sulfuric acid (12 ml) was added with 2-(2,3-dimethoxyphenyl)ethan-2-ol (10.06 g, 55.3 mmol) and left under stirring at room temperature for 15 min. After that the mixture was extracted with ethyl ether and washed successively with a 5percent potassium carbonate solution (2*150 ml) and with a sodium chloride saturated solution (1*100 ml). The solvent was dried and evaporated under reduced pressure to obtain a residue which was purified by distillation under high vacuum. At a pressure of 0.3 torr and at a temperature of 85° C., 6.47 g of the title compound distiled (65percent yield). 1 H N.M.R. (300 MHz, CDCl3) delta ppm: 2.62 (s, 3H); 3.88 (s, 3H); 3.90 (s, 3H); 7.05-7.10 (sc, 2H); 7.21 (dd, 1H).
  • 2
  • [ 6848-73-3 ]
  • diluted Cr2O3-H2SO4 [ No CAS ]
  • [ 38480-94-3 ]
 

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