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Chemical Structure| 7038-75-7 Chemical Structure| 7038-75-7

Structure of 7038-75-7

Chemical Structure| 7038-75-7

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Product Details of [ 7038-75-7 ]

CAS No. :7038-75-7
Formula : C7H8N2O
M.W : 136.15
SMILES Code : OC1=NC=NC(C2CC2)=C1
MDL No. :MFCD12032878
InChI Key :ZCBSUUFNOFEDES-UHFFFAOYSA-N
Pubchem ID :135668178

Safety of [ 7038-75-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 7038-75-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7038-75-7 ]

[ 7038-75-7 ] Synthesis Path-Downstream   1~3

  • 1
  • formimidamide acetate [ No CAS ]
  • [ 32249-35-7 ]
  • [ 7038-75-7 ]
YieldReaction ConditionsOperation in experiment
With sodium methylate; In methanol; at 16℃; for 48h; A mixture of AG-1 (50.0 g, 0.35 mol), CHN2H3.AcOH (73 g, 0.70 mol) and NaOMe (133.0 g, 2.4 mol) in MeOH (1.5 L) is stirred at 16 C for 2 days. The reaction mixture is acidified to pH7 with acetic acid and filtered. The filtrate iss concentrated under reduced pressure and the crude product is purified by chromatography on silica gel to yield intermediate AG-2.
  • 2
  • [ 32249-35-7 ]
  • [ 3473-63-0 ]
  • [ 7038-75-7 ]
YieldReaction ConditionsOperation in experiment
With sodium methylate; In methanol; at 16℃; for 48h; A mixture of AD-1 (100.0 g, 0.70 mol), formamidine acetate (146 g, 1.4 mol) and NaOMe (266.0 g, 4.9 mol) in MeOH (2 L) is stirred at 16 C for 2 days. The reaction mixture is neutralized to pH 7 with acetic acid and filtered. The filtrate is concentrated under reduced pressure and the crude product is purified by Si02 flash chromatography to yield AD-2.
  • 3
  • [ 32249-35-7 ]
  • [ 463-52-5 ]
  • [ 7038-75-7 ]
YieldReaction ConditionsOperation in experiment
With sodium methylate; In methanol; at 16℃; for 48h; Stir AD-1 (100.0 g, 0.70 mol) at 16 C,Formamidine acetate (146 g, 1.4 mol)And a mixture of NaOMe (266.0 g, 4.9 mol) in MeOH (2 L) for 2d.The reaction mixture was neutralized to pH 7 with acetic acid and filtered.The filtrate was concentrated under reduced pressure and the crude product was purified by flash chromatography from SiO2 to yield AD-2
 

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