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Chemical Structure| 7071-86-5 Chemical Structure| 7071-86-5

Structure of 7071-86-5

Chemical Structure| 7071-86-5

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Product Details of [ 7071-86-5 ]

CAS No. :7071-86-5
Formula : C14H12O2
M.W : 212.24
SMILES Code : OC1C2=C(C3=C1C=CC=C3)C(CO)=CC=C2

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Application In Synthesis of [ 7071-86-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7071-86-5 ]

[ 7071-86-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6223-83-2 ]
  • [ 7071-86-5 ]
YieldReaction ConditionsOperation in experiment
12.4 g (88.5%) In tetrahydrofuran; 9-Hydroxyfluorene-4-methanol A solution of <strong>[6223-83-2]9-fluorenone-4-carboxylic acid</strong> (14.8 g, 66 mmol) in 250 mL of THF, at 0 C was charged with a solution of 1M borane-THF complex in THF (150 mL, 150 mmol). The temperature was slowly elevated to room temperature. After 1.5 hr at room temperature the reaction was quenched with water. The reaction mixture was diluted with EtOAc. The organic layer was washed with water (*3), dried over magnesium sulfate and evaporated. Recrystallization from ether with traces of EtOAc afforded 12.4 g (88.5%) of the diol.
 

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