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Product Details of [ 708-75-8 ]

CAS No. :708-75-8 MDL No. :MFCD00012137
Formula : C7H7N5O Boiling Point : -
Linear Structure Formula :- InChI Key :UDOGNMDURIJYQC-UHFFFAOYSA-N
M.W : 177.16 Pubchem ID :135416532
Synonyms :

Safety of [ 708-75-8 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P313-P337+P313-P362-P403+P233-P405-P501 UN#:
Hazard Statements:H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 708-75-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 708-75-8 ]

[ 708-75-8 ] Synthesis Path-Downstream   1~60

  • 1
  • [ 67-56-1 ]
  • [ 1004-75-7 ]
  • [ 513-88-2 ]
  • [ 708-75-8 ]
  • 2
  • [ 13040-58-9 ]
  • [ 708-75-8 ]
  • (2-amino-6-methyl-4-oxo-4,8-dihydro-3<i>H</i>-pteridin-7-yliden)-(2-amino-4-oxo-3,4-dihydro-pteridin-7-yl)-methane [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sulfuric acid unter Zutritt von Luft;
  • 3
  • [ 708-75-8 ]
  • [ 611-55-2 ]
  • (2-amino-6-methyl-4-oxo-3,4-dihydro-pteridin-7-yl)-(2-amino-6-methyl-4-oxo-4,8-dihydro-3<i>H</i>-pteridin-7-ylidene)-methane [ No CAS ]
  • 5
  • [ 708-75-8 ]
  • [ 107-13-1 ]
  • [ 114205-18-4 ]
YieldReaction ConditionsOperation in experiment
With pyridine
  • 6
  • [ 708-75-8 ]
  • [ 4896-36-0 ]
  • 8
  • [ 708-75-8 ]
  • [ 17377-13-8 ]
YieldReaction ConditionsOperation in experiment
bei der elektrochemischen Reduktion an einer Quecksilber-Kathode;
  • 10
  • [ 708-75-8 ]
  • [ 942-41-6 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide Hydrogenation;
With hydrogen; benzenesulfonic acid In methanol at 70℃; for 15h; C29 Example C29; 8.12 mg of [Rh(COD)2]BF4 (20 μmoles) and 15.57 mg of BINAP (25 μmoles) are weighed, degassed and dissolved in a mixture of tetrahydrofuran and methanol. The solvents are condensed off under a high vacuum and the residue is taken up in 5 ml of methanol. A suspension of 0.35 g of 6-methylpterin (2 mmoles) (prepared as per P. Waring et al., Aust. J. Chem. vol. 38, page 629, 1985) and 0.32 g of benzene sulphonic acid (2 mmoles) in 25 ml of methanol is added to the catalyst. The mixture is added in a nitrogen countercurrent to a 100 ml autoclave and hydrogenated at 70° C. and 80 bars hydrogen pressure for 15 hours. The conversion rate to 6-methyl-5,6,7,8-tetrahydropterin is 63% and is determined by HPLC direct from the reaction solution. The HPLC method employed is the same one as is used for the quantitative determination of the tetrahydrofolic acid.
  • 11
  • [ 708-75-8 ]
  • [ 3116-65-2 ]
YieldReaction ConditionsOperation in experiment
With formic acid; platinum Hydrogenation.und Behandeln des Reaktionsgemisches mit Acetanhydrid;
  • 12
  • [ 708-75-8 ]
  • 2-amino-6-dibromomethyl-3<i>H</i>-pteridin-4-one; hydrobromide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With water; hydrogen bromide; bromine
  • 13
  • [ 708-74-7 ]
  • [ 623-11-0 ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
unter Ausschluss von Luft;
  • 14
  • [ 708-74-7 ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; water
  • 15
  • [ 120568-20-9 ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
at 280℃;
  • 16
  • 1-(2-amino-4-oxo-3,4-dihydro-pteridin-6-ylmethyl)-pyridinium; iodide [ No CAS ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; zinc und anschliessend mit wss.H2O2;
  • 17
  • [ 57-55-6 ]
  • 2,5,6-triaminopyrimidin-4(3H)-one sulfate [ No CAS ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
80% With sodium hydrogensulfite; sodium sulfite In water at 0 - 20℃; for 13h;
  • 20
  • [ 708-75-8 ]
  • C7H4(2)H5N5O*2Cl(2)H [ No CAS ]
YieldReaction ConditionsOperation in experiment
87% With sodium dithionite; deuteriated sodium hydroxide In water-d2 at 22℃; for 48h;
  • 21
  • [ 708-75-8 ]
  • C7H4(2)H7N5O*2Cl(2)H [ No CAS ]
  • C7H4(2)H7N5O*2Cl(2)H [ No CAS ]
YieldReaction ConditionsOperation in experiment
With deuterium In deuteromethanol; water-d2 at 22℃; for 48h; in neutral or weekly acidic media;
With diclazuril; deuterium In deuteromethanol; water-d2 at 22℃; for 1h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
  • 22
  • [ 19255-82-4 ]
  • [ 35011-47-3 ]
  • [ 13040-58-9 ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
With sodium disulfite In water at 80℃; for 6h; further cyclizating agents;
  • 23
  • [ 5392-28-9 ]
  • [ 79614-36-1 ]
  • [ 13040-58-9 ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
With piperidine; potassium hydroxide 1.) water, 20 deg C, 7 d, 2.) heating; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
  • 24
  • [ 102069-94-3 ]
  • [ 708-75-8 ]
  • [ 17377-13-8 ]
  • (6-R,S)-6-methyl-5,6,7,8-tetrahydropterin dihydrochloride [ No CAS ]
YieldReaction ConditionsOperation in experiment
35 % Chromat. With hydrogenchloride pH 3.0; Yields of byproduct given;
35 % Chromat. With hydrogenchloride pH 3.0;
  • 25
  • [ 113193-95-6 ]
  • [ 708-75-8 ]
  • [ 113193-97-8 ]
YieldReaction ConditionsOperation in experiment
1: 42% 2: 14% With aluminum-mercury amalgam; ammonia In methanol; water for 10h; Ambient temperature;
  • 26
  • [ 116-09-6 ]
  • 4-hydroxy-2,5,6-triaminopyrimidine dihydrochloride [ No CAS ]
  • [ 13040-58-9 ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
Yield given. Multistep reaction;
YieldReaction ConditionsOperation in experiment
Rk. mit NaOD;
Rk.MeJ,NaOH/MeOH:S.2024,2027;Rk.MeJ,MeOH:S.2025,2027;
14C-Markierung: mechanist. Untersuch.;
Rk. mit Trifluoressigsaeure u. Fluorsulfonsaeure -> Mono- u. Dikation: NMR-Spektren;
In water at 20℃; Photolysis;
With oxygen; rose bengal In water-d2 Irradiation;

YieldReaction ConditionsOperation in experiment
Tetrahydropterin 1,O2;
13a, KMnO4;
Methylglyoxal, Pyrimidindihydrochlorid 1, Hydrazin.;
Methylglyoxal-dihydrazon 18, 1-Dihydrochlorid;
Acetamid II,Br2,Bisulfitsalz I;
2,5,6-Triamino-4-hydroxypyrimidinium-sulfat;
Pyrimidin II, N,N-Diacetylaminoaceton (IX), N2H4;
Pyrimidin (III), CHOCOCH3 (IV), H2O (neben 7-Methylpterin <V>);
2-Amino-4(3H)-oxo-5-phenyl-azo-pyrimidyl-amino-aceton-hydrochlorid, elektrolytische Reduktion;
7,8-Dihydropterin,H2O2;
/BRN= 125006//MeCOCH2NHCOMe/Hydrazin/AcOH;
II + NH4OH + Pyruvaldehyd;
(III), Luftoxidation, 0.1m Na- u. K-phosphat-Lsg.;
V,Luftoxidation unter physiolog.Bed.;
Reduktion von Folsaeure;
Acetoxyaceton, 2,4,5-Triamino-6-oxo-dihydropyrimidin-dihydrochlorid;
6-Methyl-7,8-dihydro-pterin, KMnO4;

  • 29
  • [ 513-88-2 ]
  • 2,5,6-triaminopyrimidin-4(3H)-one dihydrochloride [ No CAS ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
28% for 0.0208333h; microwave irradiation;
  • 30
  • [ 96-26-4 ]
  • 2,5,6-triaminopyrimidin-4(3H)-one dihydrochloride [ No CAS ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
40% for 0.0177778h; microwave irradiation;
  • 31
  • [ 78-98-8 ]
  • 2,5,6-triaminopyrimidin-4(3H)-one dihydrochloride [ No CAS ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
70% In water at 0 - 5℃; for 0.0172222h; microwave irradiation;
  • 32
  • [ 708-75-8 ]
  • [ 4637-24-5 ]
  • [ 479414-72-7 ]
YieldReaction ConditionsOperation in experiment
71% In N,N-dimethyl-formamide at 20℃; for 3.5h;
  • 33
  • [ 708-75-8 ]
  • [ 4637-24-5 ]
  • [ 479414-70-5 ]
YieldReaction ConditionsOperation in experiment
74% In 1,4-dioxane for 3h; Heating;
  • 34
  • [ 142645-50-9 ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
62% With perchloric acid at 70 - 80℃; for 0.25h;
  • 35
  • [ 708-75-8 ]
  • [ 479414-70-5 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 71 percent / dimethylformamide / 3.5 h / 20 °C 2: 81 percent / Ph3P; diisopropyl azodicarboxylate / dioxane / 24 h / 20 °C
  • 36
  • [ 708-75-8 ]
  • 2-[(dimethylamino)methylene]amino}-6-methyl-3-[2-(4-nitrophenyl)ethyl]pteridin-4(3H)-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 71 percent / dimethylformamide / 3.5 h / 20 °C 2: 79 percent / Ph3P; diisopropyl azodicarboxylate / dioxane / 24 h / 20 °C
  • 37
  • [ 708-75-8 ]
  • [ 14508-72-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 71 percent / dimethylformamide / 3.5 h / 20 °C 2: 81 percent / Ph3P; diisopropyl azodicarboxylate / dioxane / 24 h / 20 °C 3: 71 percent / conc. aq. NH3 / methanol / 24 h / 20 °C
Multi-step reaction with 2 steps 1: 74 percent / dioxane / 3 h / Heating 2: 71 percent / conc. aq. NH3 / methanol / 24 h / 20 °C
  • 38
  • [ 708-75-8 ]
  • C7H4(2)H7N5O*2Cl(2)H [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 87 percent / Na2S2O4, NaOD / D2O / 48 h / 22 °C 2: D2 / PtO2 / D2O; various solvent(s)
  • 39
  • [ 708-75-8 ]
  • C7H4(2)H7N5O*2Cl(2)H [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 87 percent / Na2S2O4, NaOD / D2O / 48 h / 22 °C 2: D2 / PtO2 / D2O; various solvent(s)
  • 40
  • [ 708-75-8 ]
  • [ 708-74-7 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: 40 percent / 4-dimethylaminopyridine / 3 h / Heating 2: 44 percent / 4-chlorophenyl phosphorodichloridate, pyridine / 48 h / Ambient temperature 3: 96 percent / aq. NH3 / dioxane / 0.5 h / Ambient temperature 4: 89 percent / aq. NH3 / dioxane / 96 h / Ambient temperature
  • 41
  • [ 708-75-8 ]
  • [ 32363-58-9 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: acetic acid / 1.5 h / Heating 2: 84 percent / acetic acid / 24 h / 85 - 90 °C
  • 42
  • [ 708-75-8 ]
  • 6-hydroxymethylpterin [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: acetic acid / 1.5 h / Heating 2: 84 percent / acetic acid / 24 h / 85 - 90 °C 3: 95 percent / 3M HCl / 16 h / Ambient temperature
  • 43
  • [ 708-75-8 ]
  • [ 152941-77-0 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 40 percent / 4-dimethylaminopyridine / 3 h / Heating 2: 44 percent / 4-chlorophenyl phosphorodichloridate, pyridine / 48 h / Ambient temperature 3: 96 percent / aq. NH3 / dioxane / 0.5 h / Ambient temperature
  • 44
  • [ 708-75-8 ]
  • [ 152941-75-8 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 40 percent / 4-dimethylaminopyridine / 3 h / Heating 2: 44 percent / 4-chlorophenyl phosphorodichloridate, pyridine / 48 h / Ambient temperature
  • 45
  • [ 708-75-8 ]
  • [ 139199-08-9 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 2: NBS, AcOH
  • 46
  • [ 708-75-8 ]
  • [ 139199-10-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 2: NBS, AcOH
  • 47
  • [ 708-75-8 ]
  • [ 139199-09-0 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 2: NBS, AcOH
  • 48
  • [ 708-75-8 ]
  • [ 139242-64-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 2: NBS, AcOH
  • 49
  • [ 708-75-8 ]
  • [ 712-38-9 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 2: ozone / anschliessend Erwaermen mit wss. H2O2 in wss. HCl
  • 50
  • [ 708-75-8 ]
  • [ 99056-85-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: aqueous pyridine 2: NaOH; water
  • 51
  • [ 708-75-8 ]
  • [ 110181-78-7 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: aqueous pyridine 2: aqueous acetic acid
  • 52
  • [ 708-75-8 ]
  • [ 98-11-3 ]
  • [ 942-41-6 ]
YieldReaction ConditionsOperation in experiment
63% Stage #1: In tetrahydrofuran; methanol Stage #2: 2-amino-6-methylpteridin-4(1H)-one; benzenesulfonic acid With hydrogen In methanl at 70℃; for 15h; 29 Beispiel 29: 8,12 mg [Rh(COD)2]BF4 (20 umol) und 15,57 mg BINAP (25 umol) werden eingewogen, entgast und in einer Mischung aus Tetrahydrofuran und Methanol gelost. Die Losungsmittel werden im Hochvakuum abkondensiert und der Ruckstand in 5 ml Methanol aufgenommen. Zum Katalysator wird eine Suspension aus 0,35 g 6-Methylpterin (2 mmol) (hergestellt nach P. Waring et al., Aust. J. Chem., Bd. 38, Seite 629, 1985) und 0,32 g Benzolsulfonsaure (2 mmol) in 25 ml Methanol gegeben. Die Mischung wird im Stickstoffgegenstrom in einen 100 ml Autoklaven gegeben und bei 70oC und 80 bar Wasserstoffdruck 15 Stunden lang hydriert. Der Umsatz zu 6-Methyl-5,6,7,8-tetrahydropterin betragt 63% und wird mit HPLC direkt aus der Reaktionslosung bestimmt. Die verwendete HPLC-Methode ist die Gleiche, die fur die quantitative Bestimmung der Tetrahydrofolsaure verwendet wird.
  • 54
  • [ 708-75-8 ]
  • [ 97-72-3 ]
  • N-(6-methyl-4-oxo-3,4-dihydropteridin-2-yl)isobutyramide [ No CAS ]
YieldReaction ConditionsOperation in experiment
57% With pyridine for 4.5h; Reflux;
  • 55
  • [ 35011-47-3 ]
  • [ 78-98-8 ]
  • [ 708-75-8 ]
  • 56
  • [ 708-75-8 ]
  • C53H65EuN14O15(3+) [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: acetic acid / 140 °C 2: acetic acid; N-Bromosuccinimide; dibenzoyl peroxide / 3 h / 120 °C 3: calcium carbonate / N,N-dimethyl acetamide / 3 h / 95 °C / Inert atmosphere 4: tetrakis(actonitrile)copper(I) hexafluorophosphate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; <i>tert</i>-butyl alcohol / 50 °C / Inert atmosphere
  • 57
  • [ 708-75-8 ]
  • N-[6-(bromomethyl)-4-oxo-1,4-dihydropteridin-2-yl]acetamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: acetic acid / 140 °C 2: acetic acid; N-Bromosuccinimide; dibenzoyl peroxide / 3 h / 120 °C
  • 58
  • [ 708-75-8 ]
  • (S)-4-[N-(2-acetamido-4-oxo-3,4-dihydropteridin-6-yl)methyl-(N-propargyl)amino]benzoylglutamic acid diethylester [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: acetic acid / 140 °C 2: acetic acid; N-Bromosuccinimide; dibenzoyl peroxide / 3 h / 120 °C 3: calcium carbonate / N,N-dimethyl acetamide / 3 h / 95 °C / Inert atmosphere
  • 59
  • [ 708-75-8 ]
  • [ 97-72-3 ]
  • [ 79-31-2 ]
  • N-(6-methyl-4-oxo-3,4-dihydropteridin-2-yl)isobutyramide [ No CAS ]
YieldReaction ConditionsOperation in experiment
62% With dmap at 80℃; for 2h; 1.2 Synthesis of N- (6-methyl-4-oxo-3,4-dihydropteridin-2-yl) isobutyramide (1-b) Isobutyric anhydride (10 mL) and N, N-dimethyl-4-aminopyridine (DMAP) (0.5 g) are added to a solution of compound (1-a) (4.71 g) in isobutyric acid (100 mL), and 80 ° C. Stir at for 2 hours and filter the clear solution. The filtrate was cooled to room temperature and left for 3 hours. The crystals were collected, washed with ethyl acetate and evaporated to dryness to give compound (1-b) (4.08 g, yield 62%) as a red solid.
  • 60
  • [ 1004-75-7 ]
  • [ 78-98-8 ]
  • [ 708-75-8 ]
YieldReaction ConditionsOperation in experiment
80% Stage #1: 2,5,6-triamino-4-hydroxypyrimidine With sodium sulfite In water Stage #2: 2-oxopropanal With sodium hydrogensulfite In water at 5 - 20℃; 1.1 Synthesis of 2-amino-6-methylpteridin-4 (3H) -one (1-a) Sodium sulfite (96.0 g) in a suspension of 3,5,6-triamino-4-hydroxypyrimidine (8 g) and water (800 mL)Was added and stirred. It was cooled to 0-5 ° C. when the mixture became a clear solution.A 30% aqueous solution of 2-oxopropanal (8 g) and a solution of sodium bisulfite (3.8 g) and water (80 mL) were added dropwise over 40 minutes and kept at 5 ° C. The mixture was stirred at room temperature overnight. The yellow solid is collected by filtration, washed with water, ethanol and evaporated to dryness under reduced pressure as a yellow solid4.72 g (yield 80%) of 2-amino-6-methylpteridin-4 (3H) -one (1-a) were obtained.
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