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CAS No. : | 718-08-1 | MDL No. : | MFCD03844818 |
Formula : | C12H14O3 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | BOZNWXQZCYZCSH-UHFFFAOYSA-N |
M.W : | 206.24 | Pubchem ID : | 225855 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
31% | With piperidine; acetic acid; In benzene;Reflux; Dean-Stark; | General procedure: A solution of keto ester 5a-e (2 mmol) in anhydrous benzene (10 ml) was treated with the corresponding aldehyde (4 mmol), piperidine (0.04 ml, 0.4 mmol), and acetic acid (0.11 ml, 2 mmol), and refluxed for 1-5 h in a flask with Dean-Stark trap. After the reaction was finished (control by TLC), the reaction mixture was evaporated under vacuum and purified by column chromatography. |
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