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Chemical Structure| 71869-80-2 Chemical Structure| 71869-80-2

Structure of 71869-80-2

Chemical Structure| 71869-80-2

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Product Details of [ 71869-80-2 ]

CAS No. :71869-80-2
Formula : C13H13NO5
M.W : 263.25
SMILES Code : O=C(OCC1=CC=CC=C1)N[C@H](CCC(O2)=O)C2=O

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Application In Synthesis of [ 71869-80-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 71869-80-2 ]

[ 71869-80-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 71869-80-2 ]
  • [ 77497-95-1 ]
  • [ 97975-49-0 ]
  • 2
  • [ 63648-73-7 ]
  • [ 71869-80-2 ]
YieldReaction ConditionsOperation in experiment
100% With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20℃; for 20h;Inert atmosphere; To a stirred solution of Z-D-Glu(OH)-OH (1 eq) in anhydrous THF (10 vols) under argon was added DCC (1 eq) and the reaction mixture was allowed to stir at r. t. for 20 h. The precipitate was filtered, washed with anhydrous THF (2 x 3 mL) and the solution was concentrated to dryness to afford the title compound as a viscous oil (510 mg, quant.).1H NMR (CDCl3, 300 MHz) δ 1.88-2.05 (m, 1H), 2.38-2.53 (m, 1H), 2.80-2.97 (m, 1H), 3.04 (ddd, J = 18.6, 5.4, 1.8 Hz, 1H), 4.45 (m, 1H), 5.14 (s, 2H), 5.63 (br s, 1H), 7.27-7.43 (m, 5H).
 

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