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Chemical Structure| 72000-67-0 Chemical Structure| 72000-67-0

Structure of 72000-67-0

Chemical Structure| 72000-67-0

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Product Details of [ 72000-67-0 ]

CAS No. :72000-67-0
Formula : C10H6BrNO2
M.W : 252.06
SMILES Code : O=C(C(Br)=C1)N(C2=CC=CC=C2)C1=O
MDL No. :MFCD11983355
InChI Key :XPWBLMOTTABVDZ-UHFFFAOYSA-N
Pubchem ID :351870

Safety of [ 72000-67-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 72000-67-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 72000-67-0 ]

[ 72000-67-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 5926-51-2 ]
  • [ 62-53-3 ]
  • [ 72000-67-0 ]
YieldReaction ConditionsOperation in experiment
66% With acetic acid; at 80℃; for 3h; General procedure: 3-Bromomaleic anhydride (1.0 equiv, 5.65 mmol, 1.0 g) wasdissolved in AcOH (20 mL). Methylamine hydrochloride(1.0 equiv, 5.65 mmol, 0.37 g) was then added, and thereaction was heated at 80 °C for 3 h. Solvent was removed invacuo, and the crude mixture was purified by columnchromatography over silica gel (EtOAc?hexane 0?30percent)using an ISCOTM purification system to afford 0.97 g of awhite solid (90percent yield).
 

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Technical Information

• Acyl Group Substitution • Alkyl Halide Occurrence • Baeyer-Villiger Oxidation • Barbier Coupling Reaction • Baylis-Hillman Reaction • Bucherer-Bergs Reaction • Chan-Lam Coupling Reaction • Clemmensen Reduction • Complex Metal Hydride Reductions • Corey-Bakshi-Shibata (CBS) Reduction • Corey-Chaykovsky Reaction • Fischer Indole Synthesis • General Reactivity • Grignard Reaction • Henry Nitroaldol Reaction • Hiyama Cross-Coupling Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Kinetics of Alkyl Halides • Kumada Cross-Coupling Reaction • Lawesson's Reagent • Leuckart-Wallach Reaction • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Peterson Olefination • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Aldehydes and Ketones • Preparation of Amines • Prins Reaction • Reactions of Aldehydes and Ketones • Reactions of Alkyl Halides with Reducing Metals • Reactions of Amines • Reactions of Benzene and Substituted Benzenes • Reactions of Dihalides • Reformatsky Reaction • Robinson Annulation • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Specialized Acylation Reagents-Carbodiimides and Related Reagents • Specialized Acylation Reagents-Ketenes • Stille Coupling • Stobbe Condensation • Substitution and Elimination Reactions of Alkyl Halides • Suzuki Coupling • Tebbe Olefination • Ugi Reaction • Wittig Reaction • Wolff-Kishner Reduction

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