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[ CAS No. 72224-25-0 ]

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Product Details of [ 72224-25-0 ]

CAS No. :72224-25-0 MDL No. :MFCD24498016
Formula : C11H12O4 Boiling Point : -
Linear Structure Formula :- InChI Key :PAYGWDOCZMSKLL-UHFFFAOYSA-N
M.W :208.21 Pubchem ID :12941050
Synonyms :

Safety of [ 72224-25-0 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 72224-25-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 72224-25-0 ]

[ 72224-25-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 72224-22-7 ]
  • [ 72224-25-0 ]
YieldReaction ConditionsOperation in experiment
With N-Bromosuccinimide; citric acid; In sodium hydroxide; water; acetone; Method B A solution of 2.00 g (10.4 mmol) of 4-allyloxyphenylacetic acid and 1.6 g. of NBS in 10 ml. of acetone and 4 ml. of water was stirred 30 minutes at 0 and allowed to warm to room temperature. After an hour 0.2 g of NBS were added and after a total of 2.5 hour, the mixture was cooled in an ice bath and 5.5 ml of 4 N sodium hydroxide were added. The mixture was warmed to room temperature, stirred one hour, and diluted with water, ice, and 10% citric acid solution. The solution was extracted with methylene chloride and the methylene chloride layers afforded the product as an off-white solid, m.p. 72-76.
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