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Chemical Structure| 7226-39-3 Chemical Structure| 7226-39-3

Structure of 7226-39-3

Chemical Structure| 7226-39-3

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Product Details of [ 7226-39-3 ]

CAS No. :7226-39-3
Formula : C6H11FO5
M.W : 182.15
SMILES Code : OC[C@@H]1[C@H]([C@H]([C@H](C(O1)O)F)O)O
MDL No. :N/A

Safety of [ 7226-39-3 ]

Application In Synthesis of [ 7226-39-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7226-39-3 ]

[ 7226-39-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 7226-39-3 ]
  • [ 26116-13-2 ]
  • [ 1563187-69-8 ]
YieldReaction ConditionsOperation in experiment
With sodium acetate; acetic acid; aniline; In water; at 20.0℃; for 4.0h;pH 4.2; FDG<strong>[26116-13-2]NAP</strong>: To synthesize FDG<strong>[26116-13-2]NAP</strong>, 7 mul (5.50×10-5 mole) of <strong>[26116-13-2]NAP</strong> and 5.0 mg (2.75×10-5 mole) FDG were dissolved in 0.2 mL acetate buffer (0.1M sodium acetate-acetic acid, pH4.2) and 5 mul aniline as a catalyst. The solution was left at room temperature for 4 hrs. Preparatory TLC was performed using 9:1 dichloromethane-methanol to provide FDG<strong>[26116-13-2]NAP</strong> in 31% yield MS: m/z 305 [M+H]+. Aniline used as a catalyst also showed small amounts (approx. 20-30%) of the FDG adduct (MS: m/z 280 [M+Na]+.
 

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