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Chemical Structure| 72625-07-1 Chemical Structure| 72625-07-1

Structure of 72625-07-1

Chemical Structure| 72625-07-1

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Product Details of [ 72625-07-1 ]

CAS No. :72625-07-1
Formula : C21H25NO6S
M.W : 419.49
SMILES Code : O=C(C1=C(NC(C2=CC(OC)=C(OC)C(OC)=C2)=O)SC3=C1CCCC3)OCC

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Application In Synthesis of [ 72625-07-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 72625-07-1 ]

[ 72625-07-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 14779-17-0 ]
  • [ 72625-07-1 ]
  • [ 1448530-42-4 ]
YieldReaction ConditionsOperation in experiment
65% With phosphorus pentoxide; trichlorophosphate; for 5h;Reflux; General procedure: To a solution of 2a,b (5 mmol) in phosphorus oxychloride (10 ml) was added a solution of the appropriate amine (5 mmol) and phosphorus pentoxide (5 mmol) in phosphorus oxychloride (5 ml), and the mixture was refluxed for 5 h. After cooling, the reaction mixture was poured onto ice/water and neutralized with 5% sodium hydroxide solution; the formed precipitate was filtered, washed with water and crystallized from the ethanol.
  • 2
  • [ 72625-07-1 ]
  • [ 73458-39-6 ]
  • [ 1448530-43-5 ]
YieldReaction ConditionsOperation in experiment
91% With phosphorus pentoxide; trichlorophosphate; for 5h;Reflux; General procedure: To a solution of 2a,b (5 mmol) in phosphorus oxychloride (10 ml) was added a solution of the appropriate amine (5 mmol) and phosphorus pentoxide (5 mmol) in phosphorus oxychloride (5 ml), and the mixture was refluxed for 5 h. After cooling, the reaction mixture was poured onto ice/water and neutralized with 5% sodium hydroxide solution; the formed precipitate was filtered, washed with water and crystallized from the ethanol.
 

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