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[ CAS No. 72678-02-5 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 72678-02-5
Chemical Structure| 72678-02-5
Structure of 72678-02-5 * Storage: {[proInfo.prStorage]}
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Product Details of [ 72678-02-5 ]

CAS No. :72678-02-5 MDL No. :MFCD11848605
Formula : C10H10N2O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 174.20 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 72678-02-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 72678-02-5 ]

[ 72678-02-5 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 573-54-6 ]
  • [ 72678-02-5 ]
  • [ 369652-59-5 ]
  • 2
  • [ 58142-97-5 ]
  • [ 72678-02-5 ]
  • 3
  • [ 58142-97-5 ]
  • [ 72678-03-6 ]
  • [ 72678-02-5 ]
YieldReaction ConditionsOperation in experiment
0.32 g (27%) With sodium; In methanol; EXAMPLE XXII 1-Methoxy-5-isoquinolinamine To a solution of 1.0 g of sodium (43.4 mmol) in methanol was added 1.42 g (6.8 mmol) of <strong>[58142-97-5]1-chloro-5-nitroisoquinoline</strong>. The mixture was heated under reflux for three hours, cooled, and concentrated. The residue was partitioned between water and methylene chloride, dried, and filtered through SiO2. The filtrate was concentrated to give 1.3 g of the 1-methoxy-5-nitroisoquinoline. This material was suspended in 150 ml of methanol, 0.3 g of 5% Pd-C was added, and the mixture was hydrogenated at room temperature for 18 hours. The mixture was filtered and concentrated. The residue was crystallized from ether/hexane to give 0.32 g (27%) of the desired product; mp 53-57.
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