Home Cart Sign in  
Chemical Structure| 73415-85-7 Chemical Structure| 73415-85-7

Structure of 73415-85-7

Chemical Structure| 73415-85-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 73415-85-7 ]

CAS No. :73415-85-7
Formula : C12H16N2O
M.W : 204.27
SMILES Code : O=C(C1CCNCC1)NC2=CC=CC=C2
MDL No. :MFCD07366321

Safety of [ 73415-85-7 ]

Application In Synthesis of [ 73415-85-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 73415-85-7 ]

[ 73415-85-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 3034-31-9 ]
  • [ 73415-85-7 ]
YieldReaction ConditionsOperation in experiment
In chloroform; acetic acid; PREPARATION A Preparation of 4-(N-phenylcarbamoyl)piperidine 4-(N-phenylcarbamoyl)pyridine [75.0 g, prepared as in Chem. Abs., 2013h (1958)] was hydrogenated in acetic acid (800 ml) using a platinum oxide catalyst at 50 p.s.i./30. The catalyst was then removed by filtration, the solution evaporated, the residue basified to about pH 12 with sodium hydroxide, extracted with chloroform, and the organic extract discarded. The aqueous phase was evaporated to dryness, the residue boiled with chloroform, filtered and evaporated to leave 4-(N-phenylcarbamoyl)piperidine (17.0 g), m.p. 121-127. The hydrochloride salt, m.p. 231-233, was prepared in isopropanol from the free base and hydrogen chloride, and was recrystallized from isopropanol/ethyl acetate. Analysis %: Found: C, 60.1; H, 7.2; N, 11.7. Calculated for C12 H16 N2 O.HCl: C, 59.9; H, 7.1; N, 11.6.
 

Historical Records

Technical Information

Categories