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Chemical Structure| 7404-35-5 Chemical Structure| 7404-35-5

Structure of 7404-35-5

Chemical Structure| 7404-35-5

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Product Details of [ 7404-35-5 ]

CAS No. :7404-35-5
Formula : C14H20O9
M.W : 332.30
SMILES Code : O=C(C)O[C@H]1[C@H](OC(C)=O)[C@@H](C)O[C@H](OC(C)=O)[C@@H]1OC(C)=O

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Application In Synthesis of [ 7404-35-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7404-35-5 ]

[ 7404-35-5 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 2478-38-8 ]
  • [ 108-24-7 ]
  • [ 24332-96-5 ]
  • [ 28294-47-5 ]
  • [ 7404-35-5 ]
  • [ 141243-24-5 ]
  • 2
  • [ 108-24-7 ]
  • [ 24332-96-5 ]
  • [ 498-02-2 ]
  • [ 54771-60-7 ]
  • [ 7404-35-5 ]
  • [ 141243-23-4 ]
  • 3
  • [ 38240-29-8 ]
  • [ 7404-35-5 ]
  • C11H14N2O6S [ No CAS ]
  • 4
  • [ 38240-29-8 ]
  • [ 7404-35-5 ]
  • C17H20N2O9S [ No CAS ]
YieldReaction ConditionsOperation in experiment
60% With scandium(III) chloride; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; at 40℃; for 5.0h;Inert atmosphere; Ionic liquid; Sealed tube; Microwave irradiation; Weigh 0.30 g ScCl3, 0.33 g of tetraacetylated fucose, 0.155 g of <strong>[38240-29-8]3-nitro-2-mercaptopyridine</strong> ,In parallel reaction tube. Under an atmosphere of nitrogen ionic liquid PFIL-5 [R1, R2 = ethoxy, n = 3, X = (CF3SO2) 2N] 2mL and the general ionic liquid 3-butyl-1-methylimidazolium hexafluorophosphate 2mL, Closed reaction tube, Stirring reaction, Microwave irradiation using intermittent, Power 350W, Each irradiation for 5 minutes, Stop irradiation for 1 minute. Reaction for 5 hours, Temperature control at 40 degrees Celsius. The reaction was terminated by adding water. After silica gel column separation, 0.256 g of glycoside 1-1 was obtained, Yield 60% .Ionic liquids can be reused, Yield no significant change.
 

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