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Chemical Structure| 741705-00-0 Chemical Structure| 741705-00-0

Structure of 741705-00-0

Chemical Structure| 741705-00-0

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Product Details of [ 741705-00-0 ]

CAS No. :741705-00-0
Formula : C12H15NO3S
M.W : 253.32
SMILES Code : O=CC1=CC=C(S(=O)(N2CCCCC2)=O)C=C1

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Application In Synthesis of [ 741705-00-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 741705-00-0 ]

[ 741705-00-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 741705-00-0 ]
  • [ 57497-39-9 ]
  • [ 862499-66-9 ]
YieldReaction ConditionsOperation in experiment
Example 28 N-(tert-Butyl)-C-[4-(piperidine-1-sulfonyl)phenyl]nitrone (28) The title compound was prepared according to the procedure described in Example 23, starting from <strong>[57497-39-9]N-tert-butylhydroxylamine hydrochloride</strong> and 4-(piperidine-1-sulfonyl) benzaldehyde MS: m/z 325 (MH+).
  • 2
  • [ 110-89-4 ]
  • [ 85822-16-8 ]
  • [ 741705-00-0 ]
YieldReaction ConditionsOperation in experiment
988 mg With N-ethyl-N,N-diisopropylamine; In chloroform; at 20℃; To the 4 - sulphur chloride of acid [...] 818 mg chloroform 20 ml solution is added diisopropyl trifluoroethylamine 1.4 ml, then add piperidine 394 mul, stirring at room temperature overnight. The addition of water, the chloroform layer washing 2 times. Then the saturated salt water for washing, for magnesium sulfate drying, filtering, the distill goes solvent under reduced pressure, to obtain the title compound 988 mg.
 

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