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Chemical Structure| 75449-34-2 Chemical Structure| 75449-34-2

Structure of 75449-34-2

Chemical Structure| 75449-34-2

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Product Details of [ 75449-34-2 ]

CAS No. :75449-34-2
Formula : C10H7N3
M.W : 169.18
SMILES Code : C12=NC=CC=C1NC3=CC=CN=C32

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Application In Synthesis of [ 75449-34-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 75449-34-2 ]

[ 75449-34-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 870119-58-7 ]
  • [ 75449-34-2 ]
  • C34H22N4 [ No CAS ]
YieldReaction ConditionsOperation in experiment
75% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; water; toluene; at 100℃; for 24h;Inert atmosphere; Compound 6 (2.73 g, 7.4 mmol), compound 48 (2 g, 6.17 mmol), was added to a 250 ml single-necked flask.30 ml of a 2 M potassium carbonate aqueous solution was dissolved in a solvent of 30 ml of ethanol and 60 ml of toluene.Under the protection of N2, Pd(PPh3)4 (1.5 g, 1.95 mmol) was added. The temperature was slowly raised to 100 C, and the mixture was reacted under reflux for 24 hours.After cooling, the layers were separated, the organic layer was evaporated, and then evaporated to afford product. Yield: 75%
 

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