Alternatived Products of [ 7549-44-2 ]
Product Details of [ 7549-44-2 ]
CAS No. : | 7549-44-2 |
MDL No. : | MFCD00185690 |
Formula : |
C14H14O4
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
246.26
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 7549-44-2 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 7549-44-2 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 7549-44-2 ]
- 1
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[ 7549-44-2 ]
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[ 4251-21-2 ]
- 2
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[ 7549-44-2 ]
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[ 14927-64-1 ]
Yield | Reaction Conditions | Operation in experiment |
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Multi-step reaction with 5 steps
1: H2 / Pd/C
2: aq. KOH
3: 65 percent / PPS / 4 h / 90 °C
4: 95 percent / H2 / Pd/C / dioxane; propan-2-ol / 18 h / 3040 - 3800 Torr
5: PPS / 5 h / 80 °C |
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- 3
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[ 7549-44-2 ]
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[ 19417-59-5 ]
Yield | Reaction Conditions | Operation in experiment |
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Multi-step reaction with 3 steps
1: H2 / Pd/C / tetrahydrofuran / 40 - 50 °C
2: LiAlH4 / tetrahydrofuran / 50 - 60 °C
3: HBr / 120 - 130 °C |
|
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Multi-step reaction with 2 steps
1: ethanol; sodium / 100 - 110 °C
2: HBr / 120 - 130 °C |
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Reference:
[1]Gleiter, Rolf; Kraemer, Rolf; Irngartinger, Hermann; Bissinger, Claus
[Journal of Organic Chemistry, 1992, vol. 57, # 1, p. 252 - 258]
[2]Ruzicka; Buijs; Stoll
[Helvetica Chimica Acta, 1932, vol. 15, p. 1220,1224]