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[ CAS No. 75853-20-2 ]

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Cat. No.: {[proInfo.prAm]}
2D
Chemical Structure| 75853-20-2
Chemical Structure| 75853-20-2
Structure of 75853-20-2 *Storage: {[proInfo.prStorage]}

Quality Control of [ 75853-20-2 ]

Related Doc. of [ 75853-20-2 ]

SDS
Alternatived Products of [ 75853-20-2 ]
Alternatived Products of [ 75853-20-2 ]

Product Details of [ 75853-20-2 ]

CAS No. :75853-20-2MDL No. :MFCD00010627
Formula : C7H6F2O Boiling Point : -
Linear Structure Formula :-InChI Key :N/A
M.W :144.12Pubchem ID :-
Synonyms :

Computed Properties of [ 75853-20-2 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 75853-20-2 ]

Signal Word:WarningClass:N/A
Precautionary Statements:P305+P351+P338UN#:N/A
Hazard Statements:H319Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 75853-20-2 ]

  • Downstream synthetic route of [ 75853-20-2 ]

[ 75853-20-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 75853-20-2 ]
  • [ 85117-99-3 ]
YieldReaction ConditionsOperation in experiment
50% With phosphorus tribromide; In dichloromethane; at 20℃; for 16h; To a solution of (2,5-difluoro-phenyl)-methanol (4.8 g, 33.6 mmol) in dichloromethane (40 mL) was added drop wise phosphorus tribromide (94 g, 33.6 mmol) .The mixture was stirred at room temperature for 16 h. The reaction was poured onto ice/water. The aqueous phase was made basic with sodium bicarbonate. The aqueous phase was extracted with <n="122"/>dichloromethane. The organic phase was concentrated under reduced pressure. The residue was purified by silica gel chromatography eluting with (hexanes/ethyl acetate 90:10) to give the title compound (3.5g, 50 %).
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