Home Cart Sign in  
Chemical Structure| 75937-17-6 Chemical Structure| 75937-17-6

Structure of 75937-17-6

Chemical Structure| 75937-17-6

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 75937-17-6 ]

CAS No. :75937-17-6
Formula : C9H19NO3S
M.W : 221.32
SMILES Code : O=C(OC(C)(C)C)NCCSCCO
MDL No. :MFCD24466246

Safety of [ 75937-17-6 ]

Application In Synthesis of [ 75937-17-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 75937-17-6 ]

[ 75937-17-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 158690-56-3 ]
  • [ 60-24-2 ]
  • [ 75937-17-6 ]
YieldReaction ConditionsOperation in experiment
10.7 g With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 20℃; step 2. 2-Mercaptoethanol (7.25 mL, 104 mmol), DBU (15.4 mL, 103 mmol), 2-(tert-butoxy-carbonylamino)ethyl 4-methylbenzenesulfonate (26 g, crude) and PhMe (200 mL) were combined in a 500 mL round bottom flask and stirred at RT overnight. The reaction mixture was washed with water and brine and dried (Na2SO4), filtered and concentrated in vacuo. The crude product was purified by SiO2 chromatography eluting with a PE/EtOAc gradient (325 to 33% EtOAc) to afford tert-butyl 2-(2-hydroxyethylthio)ethylcarbamate (10.7 g, 56% for 2 steps) as a colorless oil. TLC: Rf=0.35 (PE/EtOAc-2:1).
 

Historical Records

Technical Information

Categories