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Chemical Structure| 7625-53-8 Chemical Structure| 7625-53-8

Structure of 7625-53-8

Chemical Structure| 7625-53-8

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Product Details of [ 7625-53-8 ]

CAS No. :7625-53-8
Formula : C4H9NO2
M.W : 103.12
SMILES Code : CC(N)C(OC)=O
MDL No. :MFCD00272232

Safety of [ 7625-53-8 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H314-H225
Precautionary Statements:P501-P270-P240-P210-P233-P243-P241-P242-P264-P280-P370+P378-P303+P361+P353-P301+P330+P331-P363-P301+P312+P330-P304+P340+P310-P305+P351+P338+P310-P403+P235-P405
Class:3(8)
UN#:2924
Packing Group:

Application In Synthesis of [ 7625-53-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7625-53-8 ]

[ 7625-53-8 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 7625-53-8 ]
  • [ 35320-22-0 ]
  • 2
  • [ 7625-53-8 ]
  • [ 116986-09-5 ]
  • [ 1046121-17-8 ]
  • 3
  • [ 24424-99-5 ]
  • [ 7625-53-8 ]
  • [ 91103-47-8 ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In dichloromethane; at 0 - 23℃; for 16h; [0213] To a stirred solution of compound 11(16.0 g, 114.7 mmol, 1 eq) in CH2C12 (60 mL) was added TEA (48.1 mL, 344.1 mmol, 3 eq) and BOC-anhydride (30 g 137.6 mmol, 1.2 eq) at 0C and the resulting mixture was stirred at 23C for 16 h. The mixture was poured into ice cold water (500 mL), extracted with EtOAc (2 x 300 mL) and the combined extracts were washed with brine. The organic layer was dried over anhydrous sodium sulfate, filtered and concentrated to dryness to obtain crude title compound (20.0 g 72%) as an off white solid. 1H NMR (400 MHz, DMSO-d6) oe 7.25 (d, 1H, J = 7 Hz), 3.99 (m, 1H), 3.30 (s, 3H), 1.37 (m, 9H), 1.22 (d, 3H, J = 7 Hz).
 

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