Alternatived Products of [ 76995-87-4 ]
Product Details of [ 76995-87-4 ]
CAS No. : | 76995-87-4 |
MDL No. : | MFCD14706073 |
Formula : |
C13H13NO4
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | OKNSSRWVFHWDAP-UHFFFAOYSA-N |
M.W : |
247.25
|
Pubchem ID : | 53419655 |
Synonyms : |
|
Application In Synthesis of [ 76995-87-4 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 76995-87-4 ]
- 1
-
[ 76995-87-4 ]
-
[ 28027-15-8 ]
Yield | Reaction Conditions | Operation in experiment |
|
Stage #1: 4.8-Dimethoxychinaldinsaeuremethylester With methanol; sodium hydroxide; water at 0 - 20℃;
Stage #2: With hydrogenchloride; water In methanol |
2
15.3 g of the product was dissolved in 400 mL of MeOH, and 24.7 mL of 5 ΝΝaOHaq was dropwise added thereto at 00C, and the mixture was stirred overnight at room temperature. This was cooled to 00C, and 20.7 mL of 6 Ν HClaq was dropwise added thereto, and the reaction solution was concentrated. Water and mixed chloroform/MeOH were added to the residue, and shaken, and the EPO organic layer was separated and dried on sodium sulfate. After concentrated, MeOH and n-hexane were added to the residue, and the insoluble solid was taken out through filtration to obtain the intended compound as a pale yellow solid. |