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[ CAS No. 77123-61-6 ] {[proInfo.proName]}

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Chemical Structure| 77123-61-6
Chemical Structure| 77123-61-6
Structure of 77123-61-6 * Storage: {[proInfo.prStorage]}
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Product Details of [ 77123-61-6 ]

CAS No. :77123-61-6 MDL No. :N/A
Formula : C11H12FNO2Si Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 237.30 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 77123-61-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 77123-61-6 ]
  • Downstream synthetic route of [ 77123-61-6 ]

[ 77123-61-6 ] Synthesis Path-Upstream   1~3

  • 1
  • [ 77123-61-6 ]
  • [ 18761-31-4 ]
YieldReaction ConditionsOperation in experiment
60% With sodium acetate In N,N-dimethyl-formamide at 100℃; for 16 h; Step 1c.
5-Nitrobenzofuran (Compound 104)
A mixture of compound 103 (7.30 g, 30.8 mmol), sodium acetate (10.1 g, 123 mmol) and N,N-dimethylformamide (70 mL) was stirred and heated to 100° C. for 16 hours.
The precipitate was filtered and washed with N,N-dimethylformamide.
The combined filtrate was evaporated to leave a residue which was purified through a short silica gel column (eluant: ethyl acetate/petroleum ether=1/10) to provide the title compound 104 as a brown solid (3.0 g, 60percent).
Reference: [1] Patent: US2009/76044, 2009, A1, . Location in patent: Page/Page column 25
  • 2
  • [ 77123-61-6 ]
  • [ 77123-60-5 ]
Reference: [1] Journal of Organic Chemistry, 1981, vol. 46, # 11, p. 2280 - 2286
[2] Patent: JP5680638, 2015, B2,
[3] Patent: US2009/111772, 2009, A1,
  • 3
  • [ 77123-61-6 ]
  • [ 343866-99-9 ]
Reference: [1] Patent: WO2005/35520, 2005, A1, . Location in patent: Page/Page column 60
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