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Chemical Structure| 77995-54-1 Chemical Structure| 77995-54-1

Structure of 77995-54-1

Chemical Structure| 77995-54-1

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Product Details of [ 77995-54-1 ]

CAS No. :77995-54-1
Formula : C11H14N4S
M.W : 234.32
SMILES Code : CC1=NC(NN)=C(C2=C(CCCC2)S3)C3=N1
MDL No. :MFCD00449101

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Application In Synthesis of [ 77995-54-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 77995-54-1 ]

[ 77995-54-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 81765-97-1 ]
  • [ 77995-54-1 ]
YieldReaction ConditionsOperation in experiment
67% With hydrazine hydrate; In methanol; water; for 8.0h;Reflux; General procedure: The different 4-chloro-thieno[2,3-d]pyrimidine (7a-d or f-i) (1 eq.) was suspended in MeOH (5.1mL/mmol eq.) and hydrazine hydrate 80percent in water (2 eq.) and the mixture was refluxed for 5 h. Immediately after, hydrazine hydrate (2 eq.) was added to complete the reaction and the mixture was allowed to reflux for further 3 h. The reaction mixture was then cooled to r.t and placed in a fridge o.n. The resulting precipitate was filtered and crystallised from a solution of 40percent EtOH in water unless otherwise stated.
 

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