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Chemical Structure| 78465-85-7 Chemical Structure| 78465-85-7

Structure of 78465-85-7

Chemical Structure| 78465-85-7

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Product Details of [ 78465-85-7 ]

CAS No. :78465-85-7
Formula : C10H6Cl2N2S2
M.W : 289.20
SMILES Code : ClC1=CN=C(C=C1)SSC2=NC=C(C=C2)Cl

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Application In Synthesis of [ 78465-85-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 78465-85-7 ]

[ 78465-85-7 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 4214-79-3 ]
  • [ 78465-85-7 ]
  • 2
  • [ 78465-85-7 ]
  • [ 171408-84-7 ]
  • C35H20Cl2N2S2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With n-butyllithium; In tetrahydrofuran; for 0.5h;Cooling with ice; A mixed solution of Br2 / CH3COOH was added dropwise to a reaction flask equipped with 1 mol of A, and bromine was added under nitrogen atmosphereGeneration reaction. Then, bis-pyridine-substituted disulfide compound Pycl-S-S-Pycl was added, and n-BuLi / THF was used as the catalystAnd the mixture was sufficiently stirred for half an hour in a low temperature dry ice bath to give compound C. Finally, the meta-chlorobenzoic acid mCPBA /CH2Cl2, and the mixture was stirred for 1 hour. Water was added to precipitate a solid, washed with n-hexane and ethanol.Crystallization gave SDF-DPySOCl2 in 43percent yield.
  • 3
  • [ 1480-65-5 ]
  • [ 78465-85-7 ]
 

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