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[ CAS No. 82762-56-9 ] {[proInfo.proName]}

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Chemical Structure| 82762-56-9
Chemical Structure| 82762-56-9
Structure of 82762-56-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 82762-56-9 ]

CAS No. :82762-56-9 MDL No. :MFCD07439740
Formula : C9H10BrNO2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :244.09 Pubchem ID :-
Synonyms :

Safety of [ 82762-56-9 ]

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Application In Synthesis of [ 82762-56-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 82762-56-9 ]

[ 82762-56-9 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 82762-56-9 ]
  • [ 57-13-6 ]
  • [ 82762-57-0 ]
YieldReaction ConditionsOperation in experiment
22% at 150℃; for 2h;
  • 2
  • [ 89-50-9 ]
  • [ 82762-56-9 ]
YieldReaction ConditionsOperation in experiment
91% With bromine In acetic acid at 20℃; for 0.05h;
YieldReaction ConditionsOperation in experiment
2-Aethylamino-benzoesaeure, Brom, Nitrobenzol;
  • 4
  • [ 82762-56-9 ]
  • [ 82762-58-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 22 percent / 2 h / 150 °C 2: 96 percent / K2CO3 / 6 h / Heating
  • 5
  • [ 82762-56-9 ]
  • [ 82762-59-2 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 22 percent / 2 h / 150 °C 2: 71 percent / pyridine / dimethylformamide / 2 h / Heating
  • 6
  • [ 139200-39-8 ]
  • [ 82762-56-9 ]
  • C14H17BrN2O3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 23℃; for 16h;
  • 7
  • [ 82762-56-9 ]
  • C10H17NO4*C2HF3O2 [ No CAS ]
  • C14H17BrN2O3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 23℃; for 16h; Synthesis of fragments General procedure: The fragment carboxylic acid (0.35 mmol) was dissolved in dimethylformamide (0.2 M, 1.75 mL), then 14 (42.6 mg, 0.35 mmol), HBTU (128 mg, 0.34 mmol), and HOBT (51.8 mg, 0.38 mmol) were added, followed by diisopropylethylamine (175 µL, 1.047 mmol). The reaction was stirred at 23 °C for 16 h. TLC at 16 h showed conversion to product. The reaction was quenched with H2O (5 mL) and extracted with DCM (3 x 5 mL). The combined organic layers were washed with 1 M HCl (10 mL), saturated aqueous NaHCO3 (10 mL), and saturated aqueous NaCl (10 mL). The organic layer was dried over MgSO4, filtered, and evaporated. Purification with flash column chromatography with CH3OH/CH2Cl2 ( CH3OH gradient 0 → 5 %).
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