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Chemical Structure| 830325-93-4 Chemical Structure| 830325-93-4

Structure of 830325-93-4

Chemical Structure| 830325-93-4

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Product Details of [ 830325-93-4 ]

CAS No. :830325-93-4
Formula : C24H16BrN3S
M.W : 458.37
SMILES Code : BrC1=CC=C(C2=CC=C(N(C3=CC=CC=C3)C4=CC=CC=C4)C=C2)C5=NSN=C51
MDL No. :MFCD30576285

Safety of [ 830325-93-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 830325-93-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 830325-93-4 ]

[ 830325-93-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 267221-88-5 ]
  • [ 15155-41-6 ]
  • [ 830325-93-4 ]
YieldReaction ConditionsOperation in experiment
62% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; toluene; at 88℃; for 13h;Reflux; Inert atmosphere; C6H2Br2N2S (1.266 g, 4.308 mmol), C24H26BNO2, (400 mg, 1.077 mmol), Pd(PPh3)4,A mixture of K2CO3 (12.5 ml), CH3CH2OH (12.5 ml) in toluene (25.0 ml) was stirred and heated.It was refluxed at 88 C for 13 hours under a nitrogen atmosphere.The crude product was extracted three times with dichloromethane and water.It was dried over anhydrous Na 2 SO 4 .then,Using petroleum ether and dichloromethane (4:1) as the eluent,The crude product is purified by silica gel column chromatography to give the title compound.It was a pale yellow solid (yield: 62%).
 

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