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Chemical Structure| 83342-70-5 Chemical Structure| 83342-70-5

Structure of 83342-70-5

Chemical Structure| 83342-70-5

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Product Details of [ 83342-70-5 ]

CAS No. :83342-70-5
Formula : C10H7NO2
M.W : 173.17
SMILES Code : O=CC1=CNC2=CC=CC=C2C1=O
MDL No. :N/A

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Application In Synthesis of [ 83342-70-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 83342-70-5 ]

[ 83342-70-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6964-21-2 ]
  • [ 83342-70-5 ]
  • C16H9NO2S [ No CAS ]
YieldReaction ConditionsOperation in experiment
78% With acetic anhydride; potassium carbonate; at 130℃; for 4h; General procedure: A mixture of 100.0 mg (0.58 mmol, 1.00 mol eq) 1,4-dihydro-4-oxoquinoline-3-carbaldehyde 1a together with 87.0 mg (0.639 mmol, 1.10 mol eq) of phenylacetic acid(2a) and 8.00 mg (0.639 mmol, 0.10 mol eq) of K2CO3 (abs) was stirred in 3 mL of freshly distilled Ac2O at 130 C for 4 h. After cooling the reaction mixture to rt, the solid product 3a was filtered off, washed with H2O (2 9 5 mL), Et2O (1 9 5 mL) and dried under vacuum to yield 129 mg (0.46 mmol, 80%) of 3a (Scheme 2). Here we are showing physico-chemical characteristics for the compound 3a. The characteristics for all sixteen novel compounds 3 together with their spectral figures are published in the Supporting Information.
 

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