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Chemical Structure| 84596-30-5 Chemical Structure| 84596-30-5

Structure of 84596-30-5

Chemical Structure| 84596-30-5

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Product Details of [ 84596-30-5 ]

CAS No. :84596-30-5
Formula : C12H12N2
M.W : 184.24
SMILES Code : NC1=NC(C)=C(C2=CC=CC=C2)C=C1
MDL No. :MFCD12547024

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Application In Synthesis of [ 84596-30-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 84596-30-5 ]

[ 84596-30-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 36936-23-9 ]
  • [ 98-80-6 ]
  • [ 84596-30-5 ]
YieldReaction ConditionsOperation in experiment
72% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; toluene; for 12.0h;Reflux; General procedure: 2-chloropyridine-4-boronic acid (11.5 g, 0.073 mol),1-bromonaphthalene (9.9 g, 0.061 mol), tetrakis (triphenylphosphine)Palladium (3.62 g, 0.003 mol), potassium carbonate (16.9 g, 0.122 mol)150 mL of 1,4-dioxane, 150 mL of toluene and 60 mL of distilled water were added and refluxed for 12 hours. After cooling to room temperature, extracted with ethyl acetate, and separated by column chromatography to obtain [Intermediate 2-c] 11.4 g (yield 78%
 

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