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[ CAS No. 851045-63-1 ] {[proInfo.proName]}

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3d Animation Molecule Structure of 851045-63-1
Chemical Structure| 851045-63-1
Chemical Structure| 851045-63-1
Structure of 851045-63-1 * Storage: {[proInfo.prStorage]}
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Product Details of [ 851045-63-1 ]

CAS No. :851045-63-1 MDL No. :MFCD27929847
Formula : C7H5F3INO Boiling Point : -
Linear Structure Formula :- InChI Key :VDVMGAPDTJTWDH-UHFFFAOYSA-N
M.W :303.02 Pubchem ID :68678407
Synonyms :

Safety of [ 851045-63-1 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 851045-63-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 851045-63-1 ]

[ 851045-63-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 851045-63-1 ]
  • [ 13061-96-6 ]
  • [ 851045-64-2 ]
YieldReaction ConditionsOperation in experiment
79% With cesium fluoride In 1,4-dioxane at 80℃; for 3h; 182.2 Step 2. Preparation of 4-methyl-3-trifluoromethoxyanaline. Add 1, 1-bis (diphenylphosphino) ferrocene palladium (II) chloride (0.8 g, 0.1 mmol), methyl boronic acid (1.8 g, 29.7 mmol) and cesium fluoride (5.2 g, 34.6 mmol) to a solution of 4-iodo-3-trifluoromethoxyanaline (3.0 g, 9.9 mmol) in dioxane under nitrogen. After heating at 80 °C for 3 h, cool the reaction to room temperature and dilute with ethyl acetate (100 mL) and water (100 mL). Separate the organics, wash with brine, dry over sodium sulfate, and filter. Remove the solvent under vacuum and chromatograph the crude product over silica gel using ethyl acetate/hexane (5-20%) to elute. This provides the title compound (1.5 g, 79 %) as a tan oil: MS (ES+): 192 (M+H).
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