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Chemical Structure| 85387-44-6 Chemical Structure| 85387-44-6

Structure of 85387-44-6

Chemical Structure| 85387-44-6

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Product Details of [ 85387-44-6 ]

CAS No. :85387-44-6
Formula : C13H19NO
M.W : 205.30
SMILES Code : OCC1CN(CC2=CC=CC=C2)CCC1
MDL No. :MFCD01452200

Safety of [ 85387-44-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 85387-44-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 85387-44-6 ]

[ 85387-44-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 72551-53-2 ]
  • [ 85387-44-6 ]
YieldReaction ConditionsOperation in experiment
99% (l-Benzylpipeiidin-3-yl)methanol; To a solution of ethyl l-benzylpiperidine-3-carboxylate (1.0 g) in tetrahydrofuran (10 mL) at 5C under argon was added a IM solution of lithium aluminium hydride (4.04 mL) dropwise. The mixture was stirred for 1 hour at 5C and then quenched by the dropwise addition of ethyl acetate (5 mL). The mixture was warmed to room temperature and dichloromethane (150 mL) was added followed by saturated aqueous sodium potassium tartrate (50 mL). The mixture was stirred vigorously overnight. The layers were separated EPO <DP n="192"/>and the organic layer was dried over magnesium sulfate and evaporated to give the title compound as a colourless oil (0.82 g, 99%).
 

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