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[ CAS No. 86340-94-5 ] {[proInfo.proName]}

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Chemical Structure| 86340-94-5
Chemical Structure| 86340-94-5
Structure of 86340-94-5 * Storage: {[proInfo.prStorage]}
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Product Details of [ 86340-94-5 ]

CAS No. :86340-94-5 MDL No. :MFCD09037939
Formula : C7H4INO3S Boiling Point : -
Linear Structure Formula :- InChI Key :XQKQROJYWLWDMP-UHFFFAOYSA-N
M.W : 309.08 Pubchem ID :8063362
Synonyms :

Safety of [ 86340-94-5 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 UN#:N/A
Hazard Statements:H315-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 86340-94-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 86340-94-5 ]

[ 86340-94-5 ] Synthesis Path-Downstream   1~36

YieldReaction ConditionsOperation in experiment
With diethyl ether; iodine
  • 2
  • [ 128-44-9 ]
  • [ 86340-94-5 ]
YieldReaction ConditionsOperation in experiment
Stage #1: saccharin sodium salt With water; silver nitrate Stage #2: With iodine In acetone at 20℃; for 5h;
  • 3
  • [ 7553-56-2 ]
  • [ 2673-17-8 ]
  • [ 86340-94-5 ]
  • silver(I) iodide [ No CAS ]
YieldReaction ConditionsOperation in experiment
1: >99 2: >99 In further solvent(s) solvent: cyclohexanol;;
1: >99 2: >99 In ethanol
1: >99 2: >99 In diethyl ether
In benzene
1: >99 2: >99 In cyclohexene
In chloroform
1: >99 2: >99 In 1,4-dioxane
In benzene
1: >99 2: >99 In further solvent(s) solvent: cyclohexanol;;
In chloroform
1: >99 2: >99 In diethyl ether
1: >99 2: >99 In ethanol
1: >99 2: >99 In cyclohexene
1: >99 2: >99 In 1,4-dioxane

  • 4
  • [ 109-99-9 ]
  • [ 86340-94-5 ]
  • C11H12INO4S [ No CAS ]
YieldReaction ConditionsOperation in experiment
In n-heptane
  • 5
  • [ 110-86-1 ]
  • [ 86340-94-5 ]
  • C12H9IN2O3S [ No CAS ]
YieldReaction ConditionsOperation in experiment
In n-heptane; acetic acid methyl ester
  • 6
  • [ 86340-94-5 ]
  • N-iodosaccharin hydrate [ No CAS ]
YieldReaction ConditionsOperation in experiment
With water In acetonitrile
  • 7
  • [ 86340-94-5 ]
  • [ 94-41-7 ]
  • 2-(2-iodo-3-oxo-1,3-diphenylpropyl)benzo[d]isothiazol-3(2H)-one 1,1-dioxide [ No CAS ]
YieldReaction ConditionsOperation in experiment
92% With C31H44N4O4; scandium tris(trifluoromethanesulfonate) In dichloromethane at 23℃; Molecular sieve; Darkness; Inert atmosphere; optical yield given as %de; diastereoselective reaction;
  • 8
  • [ 81-07-2 ]
  • [ 86340-94-5 ]
YieldReaction ConditionsOperation in experiment
99% With [bis(acetoxy)iodo]benzene; iodine In tetrachloromethane at 20℃; for 6h; Darkness; 4 Preparation of N-iodosaccharin in CCI4 [00163] A mixture of saccharin (1.00 g, 5.46 mmol), PhI(OAc)2 (1.10 g, 3.28 mmol), I2 (0.90 g, 3.55 mmol), and CC (20 mL) was stirred for 6 h at rt and for 1 h at 0 to 5 °C. The precipitated solid was filtered, washed on the filter with cold CC14 and dried in vacuo to give 1.67 g (99%) of N-iodosaccharin as off-white powder. 1H NMR (CD3CN) δ: 7.98 (t, = 7.9 Hz, 2H), 7.85 (m, 2H) ppm; 13C NMR (CD3CN) δ: 162.6, 139.7, 135.8, 135.4, 128.5, 126.2, 122.3 ppm.
  • 9
  • [ 110-86-1 ]
  • [ 86340-94-5 ]
  • N-iodosaccharin-pyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethyl acetate
  • 10
  • [ 108-89-4 ]
  • [ 86340-94-5 ]
  • N-iodosaccharin-4-methylpyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
In dichloromethane
  • 11
  • [ 1122-58-3 ]
  • [ 86340-94-5 ]
  • N-iodosaccharin-4-dimethylaminopyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethyl acetate
  • 12
  • [ 86340-94-5 ]
  • [ 75400-67-8 ]
  • tert-butyl-3-(1,1-dioxido-3-oxobenzo[d]isothiazol-2(3H)-yl)-1H-indole-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
30% With tetra-(n-butyl)ammonium iodide In dichloromethane at 20℃; for 19h; Irradiation; Inert atmosphere;
  • 13
  • [ 18677-55-9 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C8H11NO4 [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 14
  • [ 1131-33-5 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C11H9NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 15
  • [ 1131-48-2 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C11H9NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 16
  • [ 78500-88-6 ]
  • [ 86340-94-5 ]
  • 2C7H4INO3S*C17H13NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 17
  • [ 86340-94-5 ]
  • [ 23022-74-4 ]
  • C7H4INO3S*C23H17NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 18
  • [ 1796-86-7 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C7H9NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 19
  • [ 6890-60-4 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C7H9NO2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 20
  • [ 14906-55-9 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C7H9NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 21
  • [ 1003-73-2 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C6H7NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1 at 24.84℃;
  • 22
  • [ 23569-17-7 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C9H13NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 23
  • [ 4833-24-3 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C7H9NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 24
  • [ 65257-53-6 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C8H11NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 25
  • [ 1122-96-9 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C6H7NO2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 26
  • [ 1003-67-4 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C6H7NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 27
  • [ 1073-23-0 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C7H9NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 28
  • [ 1122-45-8 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C7H9NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 29
  • [ 3376-50-9 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C8H11NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 30
  • [ 20773-98-2 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C6H7NO2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 31
  • [ 14906-61-7 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C6H7NO2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 32
  • [ 6890-63-7 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C7H9NO3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 33
  • [ 7259-54-3 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C7H9NO3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 34
  • [ 7259-53-2 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C12H11NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 35
  • [ 20531-86-6 ]
  • [ 86340-94-5 ]
  • C7H4INO3S*C12H9NO2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
In chloroform-d1; [(2)H6]acetone at 24.84℃;
  • 36
  • [ 1122-58-3 ]
  • [ 86340-94-5 ]
  • 4-(dimethylamino)pyridine N-iodosaccharin [ No CAS ]
YieldReaction ConditionsOperation in experiment
In dichloromethane-d2
Same Skeleton Products
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