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CAS No. : | 86340-94-5 | MDL No. : | MFCD09037939 |
Formula : | C7H4INO3S | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | XQKQROJYWLWDMP-UHFFFAOYSA-N |
M.W : | 309.08 | Pubchem ID : | 8063362 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 | UN#: | N/A |
Hazard Statements: | H315-H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With diethyl ether; iodine |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Stage #1: saccharin sodium salt With water; silver nitrate Stage #2: With iodine In acetone at 20℃; for 5h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
1: >99 2: >99 | In further solvent(s) solvent: cyclohexanol;; | |
1: >99 2: >99 | In ethanol | |
1: >99 2: >99 | In diethyl ether |
In benzene | ||
1: >99 2: >99 | In cyclohexene | |
In chloroform | ||
1: >99 2: >99 | In 1,4-dioxane | |
In benzene | ||
1: >99 2: >99 | In further solvent(s) solvent: cyclohexanol;; | |
In chloroform | ||
1: >99 2: >99 | In diethyl ether | |
1: >99 2: >99 | In ethanol | |
1: >99 2: >99 | In cyclohexene | |
1: >99 2: >99 | In 1,4-dioxane |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In n-heptane |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In n-heptane; acetic acid methyl ester |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With water In acetonitrile |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
92% | With C31H44N4O4; scandium tris(trifluoromethanesulfonate) In dichloromethane at 23℃; Molecular sieve; Darkness; Inert atmosphere; optical yield given as %de; diastereoselective reaction; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
99% | With [bis(acetoxy)iodo]benzene; iodine In tetrachloromethane at 20℃; for 6h; Darkness; | 4 Preparation of N-iodosaccharin in CCI4 [00163] A mixture of saccharin (1.00 g, 5.46 mmol), PhI(OAc)2 (1.10 g, 3.28 mmol), I2 (0.90 g, 3.55 mmol), and CC (20 mL) was stirred for 6 h at rt and for 1 h at 0 to 5 °C. The precipitated solid was filtered, washed on the filter with cold CC14 and dried in vacuo to give 1.67 g (99%) of N-iodosaccharin as off-white powder. 1H NMR (CD3CN) δ: 7.98 (t, = 7.9 Hz, 2H), 7.85 (m, 2H) ppm; 13C NMR (CD3CN) δ: 162.6, 139.7, 135.8, 135.4, 128.5, 126.2, 122.3 ppm. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In ethyl acetate |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In dichloromethane |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In ethyl acetate |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
30% | With tetra-(n-butyl)ammonium iodide In dichloromethane at 20℃; for 19h; Irradiation; Inert atmosphere; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1 at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In chloroform-d1; [(2)H6]acetone at 24.84℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In dichloromethane-d2 |