Alternatived Products of [ 864068-80-4 ]
Product Details of [ 864068-80-4 ]
CAS No. : | 864068-80-4 |
MDL No. : | MFCD06740322 |
Formula : |
C10H10N2O
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | VINVOQJANISHSK-UHFFFAOYSA-N |
M.W : | 174.20 |
Pubchem ID : | 7164580 |
Synonyms : |
|
Safety of [ 864068-80-4 ]
Application In Synthesis of [ 864068-80-4 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 864068-80-4 ]
- 1
-
[ 288-13-1 ]

-
[ 57455-06-8 ]

-
[ 864068-80-4 ]
Yield | Reaction Conditions | Operation in experiment |
85% |
With potassium phosphate monohydrate; iron(III) chloride hexahydrate; trans-N,N'-dimethylcyclohexane-1,2-diamine In water at 135℃; for 24h; Inert atmosphere; |
|
- 2
-
[ 864068-80-4 ]

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C36H52ClN4P2Pd2(1+)*BF4(1-)
[ No CAS ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 4 steps
1: triphenylphosphine; ethyl tribromoacetate / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
2: acetone / 12 h / Reflux; Inert atmosphere
3: toluene / 4 h / Reflux
4: dichloromethane / 5 h / 20 °C / Inert atmosphere |
|
Reference:
[1]Bailey, Wilson D.; Luconi, Lapo; Rossin, Andrea; Yakhvarov, Dmitry; Flowers, Sarah E.; Kaminsky, Werner; Kemp, Richard A.; Giambastiani, Giuliano; Goldberg, Karen I.
[Organometallics, 2015, vol. 34, # 16, p. 3998 - 4010]
- 3
-
[ 864068-80-4 ]

-
C19H26F3N2O3PPdS
[ No CAS ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 4 steps
1: triphenylphosphine; ethyl tribromoacetate / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
2: acetone / 12 h / Reflux; Inert atmosphere
3: toluene / 4 h / Reflux
4: dichloromethane / 4 h / Darkness |
|
Reference:
[1]Bailey, Wilson D.; Luconi, Lapo; Rossin, Andrea; Yakhvarov, Dmitry; Flowers, Sarah E.; Kaminsky, Werner; Kemp, Richard A.; Giambastiani, Giuliano; Goldberg, Karen I.
[Organometallics, 2015, vol. 34, # 16, p. 3998 - 4010]
- 4
-
[ 864068-80-4 ]

-
C18H27N2OPPd
[ No CAS ]

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C36H52N4OP2Pd2
[ No CAS ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 5 steps
1: triphenylphosphine; ethyl tribromoacetate / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
2: acetone / 12 h / Reflux; Inert atmosphere
3: toluene / 4 h / Reflux
4: dichloromethane / 4 h / Darkness
5: tetrahydrofuran-d8 / 16 h |
|
Reference:
[1]Bailey, Wilson D.; Luconi, Lapo; Rossin, Andrea; Yakhvarov, Dmitry; Flowers, Sarah E.; Kaminsky, Werner; Kemp, Richard A.; Giambastiani, Giuliano; Goldberg, Karen I.
[Organometallics, 2015, vol. 34, # 16, p. 3998 - 4010]
- 5
-
[ 864068-80-4 ]

-
1-(3-(bromomethyl)phenyl)-1H-pyrazole
[ No CAS ]
Yield | Reaction Conditions | Operation in experiment |
68.5% |
With ethyl tribromoacetate; triphenylphosphine In dichloromethane at 20℃; for 0.5h; Inert atmosphere; |
|
Reference:
[1]Bailey, Wilson D.; Luconi, Lapo; Rossin, Andrea; Yakhvarov, Dmitry; Flowers, Sarah E.; Kaminsky, Werner; Kemp, Richard A.; Giambastiani, Giuliano; Goldberg, Karen I.
[Organometallics, 2015, vol. 34, # 16, p. 3998 - 4010]
- 6
-
[ 864068-80-4 ]

-
1-(3-((di-tert-butylphosphino)methyl)phenyl)-1H-pyrazole
[ No CAS ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 2 steps
1: triphenylphosphine; ethyl tribromoacetate / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
2: acetone / 12 h / Reflux; Inert atmosphere |
|
Reference:
[1]Bailey, Wilson D.; Luconi, Lapo; Rossin, Andrea; Yakhvarov, Dmitry; Flowers, Sarah E.; Kaminsky, Werner; Kemp, Richard A.; Giambastiani, Giuliano; Goldberg, Karen I.
[Organometallics, 2015, vol. 34, # 16, p. 3998 - 4010]
- 7
-
[ 864068-80-4 ]

-
C18H26ClN2PPd
[ No CAS ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 3 steps
1: triphenylphosphine; ethyl tribromoacetate / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
2: acetone / 12 h / Reflux; Inert atmosphere
3: toluene / 4 h / Reflux |
|
Reference:
[1]Bailey, Wilson D.; Luconi, Lapo; Rossin, Andrea; Yakhvarov, Dmitry; Flowers, Sarah E.; Kaminsky, Werner; Kemp, Richard A.; Giambastiani, Giuliano; Goldberg, Karen I.
[Organometallics, 2015, vol. 34, # 16, p. 3998 - 4010]
- 8
-
[ 864068-80-4 ]

-
C20H29N3PPd(1+)*BF4(1-)
[ No CAS ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 4 steps
1: triphenylphosphine; ethyl tribromoacetate / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
2: acetone / 12 h / Reflux; Inert atmosphere
3: toluene / 4 h / Reflux
4: dichloromethane / 5 h / 20 °C / Inert atmosphere |
|
Reference:
[1]Bailey, Wilson D.; Luconi, Lapo; Rossin, Andrea; Yakhvarov, Dmitry; Flowers, Sarah E.; Kaminsky, Werner; Kemp, Richard A.; Giambastiani, Giuliano; Goldberg, Karen I.
[Organometallics, 2015, vol. 34, # 16, p. 3998 - 4010]
- 9
-
[ 288-13-1 ]

-
[ 15852-73-0 ]

-
[ 864068-80-4 ]
Yield | Reaction Conditions | Operation in experiment |
78.6% |
With 1-methyl-pyrrolidin-2-one; copper(l) iodide; potassium carbonate at 210℃; for 5h; Microwave irradiation; |
|
Reference:
[1]Bailey, Wilson D.; Luconi, Lapo; Rossin, Andrea; Yakhvarov, Dmitry; Flowers, Sarah E.; Kaminsky, Werner; Kemp, Richard A.; Giambastiani, Giuliano; Goldberg, Karen I.
[Organometallics, 2015, vol. 34, # 16, p. 3998 - 4010]