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Chemical Structure| 86607-65-0 Chemical Structure| 86607-65-0

Structure of 86607-65-0

Chemical Structure| 86607-65-0

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Product Details of [ 86607-65-0 ]

CAS No. :86607-65-0
Formula : C12H10O2
M.W : 186.21
SMILES Code : O=C(C1=CC=CO1)CC2=CC=CC=C2
MDL No. :MFCD12827334

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Application In Synthesis of [ 86607-65-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 86607-65-0 ]

[ 86607-65-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 86607-65-0 ]
  • [ 178686-24-3 ]
  • [ 57-13-6 ]
  • [ 1283118-40-0 ]
YieldReaction ConditionsOperation in experiment
9% With hydrogenchloride; In ethanol; water;Reflux; [00264] A mixture of l-(furan-2-yl)-2-phenylethanone (commercially available) (420 mg, 2.26 mmol), <strong>[178686-24-3]3-ethoxy-4-hydroxy-5-nitrobenzaldehyde</strong> (433 mg, 2.05 mmol), urea (369 mg, 6.15 mmol), concentrated HC1 (0.2 mL, 2.05 mmol) in EtOH (5 mL) was refluxed overnight. Followed standard aqueous/EtOAc workup procedure, then purified by preparative HPLC to give Compound 111 (83 mg, yield 9%). 1H NMR (DMSO- d6 400 MHz): delta 10.32 (s, IH), 8.63 (s, IH), 7.60 (s, IH), 7.53 (s, IH), 7.37 (d, J = 1.6 Hz, IH), 7.21- 7.18 (m, 3H), 7.10 (d, J = 1.2 Hz, IH), 6.93-6.91 (m, 2H), 6.43 (d, J = 3.2 Hz, IH), 6.29 (d, J = 3.2 Hz, IH), 5.12 (d, J = 2.8 Hz, IH), 4.06-3.96 (m, 2H), 1.32 (t, J = 6.8 Hz, 3H); MS (ESI): m/z [M+l]+.
 

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