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Chemical Structure| 866615-76-1 Chemical Structure| 866615-76-1

Structure of 866615-76-1

Chemical Structure| 866615-76-1

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Product Details of [ 866615-76-1 ]

CAS No. :866615-76-1
Formula : C9H8F4O
M.W : 208.15
SMILES Code : CC(O)C1=CC(C(F)(F)F)=CC=C1F
MDL No. :MFCD23823066

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Application In Synthesis of [ 866615-76-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 866615-76-1 ]

[ 866615-76-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 75-16-1 ]
  • [ 146137-78-2 ]
  • [ 866615-76-1 ]
YieldReaction ConditionsOperation in experiment
3.0 M methylmagnesiumbromide (7.8 ml) was dropped, in a nitrogen atmosphere at 0 C, into the THF (30 ml) solution of 2-fluoro-5-trifluoromethyl benzaldehyde (3.0 g). After the mixture was warmed to room temperature, and was then stirred for 30 minutes, it was poured into a saturated ammonium chloride aqueous solution, and was then subjected to extraction with ethyl acetate. After its organic layer was washed with brine, and was then dried with anhydrous magnesium sulfate, it was filtered, and was then concentrated under reduced pressure to produce a crude chemical compound (58) (3.42 g).
 

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