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Chemical Structure| 86732-28-7 Chemical Structure| 86732-28-7

Structure of 86732-28-7

Chemical Structure| 86732-28-7

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Product Details of [ 86732-28-7 ]

CAS No. :86732-28-7
Formula : C7H14N2
M.W : 126.20
SMILES Code : CN1CC(CNC2)C2C1
MDL No. :MFCD09608113
InChI Key :YQURLNGUWNDBIR-UHFFFAOYSA-N
Pubchem ID :12958533

Safety of [ 86732-28-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H319
Precautionary Statements:P305+P351+P338

Application In Synthesis of [ 86732-28-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 86732-28-7 ]

[ 86732-28-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 86732-28-7 ]
  • [ 3356-89-6 ]
  • 2-methyl-5-(3-phenyl-isoxazol-5-yl)-octahydro-pyrrolo[3,4-c]pyrrole [ No CAS ]
YieldReaction ConditionsOperation in experiment
25% With 1,8-diazabicyclo[5.4.0]undec-7-ene; at 140 - 145℃; for 0.666667h; EXAMPLE 32C 2-Methyl-5-(3-phenyl-isoxazol-5-yl)-octahydro-pyrrolo[3,4-c]pyrrole The product of Example 32B (1 g, 7.9 mmol), and <strong>[3356-89-6]5-chloro-3-phenyl-isoxazole</strong> (1.4 g, 7.9 mmol) (prepared according to literature procedure: Dannhardt, G.; Obergrusberger, I. Chemiker-Zeitung 1989, 113, 109-113) in DBU (1.3 g, 8.6 mmol) were warmed to 140-145 C. for 40 min. The reaction mixture was cooled to ambient temperature, CH2Cl2 was added, and the crude material was purified by flash column chromatography (SiO2, 10% CH3OH-CH2Cl2 with 1% NH4OH) to give 0.54 g of the title compound (2.0 mmol, 25% yield) which was carried on to the next step without further purification.
 

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[ 86732-28-7 ]

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