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Chemical Structure| 869959-13-7 Chemical Structure| 869959-13-7

Structure of 869959-13-7

Chemical Structure| 869959-13-7

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Product Details of [ 869959-13-7 ]

CAS No. :869959-13-7
Formula : C14H10O2
M.W : 210.23
SMILES Code : O=CC1=CC=C(C2=CC=CC(C=O)=C2)C=C1
MDL No. :MFCD29090704

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Application In Synthesis of [ 869959-13-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 869959-13-7 ]

[ 869959-13-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 869959-13-7 ]
  • [ 6971-45-5 ]
  • C28H26N4O2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
63% With hydrogenchloride; In ethanol; water; at 80℃; for 0.5h;Inert atmosphere; To a solution of [1,1'-biphenyl]-3,4'-dicarboxaldehyde (50 mg, 0.24 mmol) in EtOH (3 mL), <strong>[6971-45-5]2-methoxyphenylhydrazine hydrochloride</strong> (104 mg, 0.59 mmol)and a catalytic amount of concentrated HCl (0.04 mL) were added. The reaction mixture wasstirred at 80 C for 30 min and the resulting solution was filtered. The residue obtained was washedwith hot EtOH (25 mL) to afford compound 9a (68 mg, 63%) as a brown solid, which wasinsoluble.
 

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