Home Cart Sign in  
Chemical Structure| 872983-77-2 Chemical Structure| 872983-77-2

Structure of 872983-77-2

Chemical Structure| 872983-77-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 872983-77-2 ]

CAS No. :872983-77-2
Formula : C13H14ClNO4S
M.W : 315.77
SMILES Code : O=C(N1C(S(=O)(Cl)=O)=CC2=C1C=CC=C2)OC(C)(C)C
MDL No. :MFCD11044967

Safety of [ 872983-77-2 ]

Application In Synthesis of [ 872983-77-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 872983-77-2 ]

[ 872983-77-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 872983-77-2 ]
  • [ 134575-12-5 ]
  • C24H33N3O6S [ No CAS ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In dichloromethane; at 20℃; for 16.0h; Step 2: A solution of amine B (0.3 g, 1.4 mmol) and triethylamine (0.99 ml_,7 mmol) in CH2CI2 (30 ml) at room temperature was treated with the indolesulfonyl chloride (5a) prepared in step 1 (0.5 g, 1.55 mmol). The mixture wasstirred for 16 h and then diluted with CH2CI2 (100 ml_) and washed once withwater (50 ml_) and twice with brine (50 ml_ each wash). The organic phase wasseparated, dried (Na2SO4) and concentrated to yield a crude product which waspurified by silica-gel chromatography using 1:1 ethyl acetate:hexane as the elutingsolvent. The appropriate fractions were collected and combined, and the solventwas removed under vacuum to provide pure product (5b) (0.46 g).
 

Historical Records