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Chemical Structure| 876299-63-7 Chemical Structure| 876299-63-7

Structure of 876299-63-7

Chemical Structure| 876299-63-7

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Product Details of [ 876299-63-7 ]

CAS No. :876299-63-7
Formula : C14H13BrO
M.W : 277.16
SMILES Code : CC1=CC(Br)=CC(OCC2=CC=CC=C2)=C1
MDL No. :MFCD28973295
InChI Key :QWFHNVJNLZJNBU-UHFFFAOYSA-N
Pubchem ID :68901598

Safety of [ 876299-63-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 876299-63-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 876299-63-7 ]

[ 876299-63-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 74204-00-5 ]
  • [ 100-39-0 ]
  • [ 876299-63-7 ]
YieldReaction ConditionsOperation in experiment
100% With potassium carbonate; In acetone; for 2.0h;Heating / reflux; A mixture of <strong>[74204-00-5]3-bromo-5-methylphenol</strong> [(40.7 g, 218 mmol) J. Amer. Chem. Soc., 2003, 125, 7792)], benzyl bromide (28.6 mL, 239 mmol) and potassium carbonate (90.2 g, 653 mmol) in acetone (1 L) was heated under reflux for 2 hours. The cooled reaction mixture was then acidified with 2M hydrochloric acid and the aqueous layer was extracted with ethyl acetate. The organic solution was washed with brine (*3), dried over magnesium sulfate and concentrated in vacuo to afford the title compound as a red oil in quantitative yield.
 

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