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Chemical Structure| 88513-00-2 Chemical Structure| 88513-00-2

Structure of 88513-00-2

Chemical Structure| 88513-00-2

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Product Details of [ 88513-00-2 ]

CAS No. :88513-00-2
Formula : C6H7N3O3
M.W : 169.14
SMILES Code : O=C(N1)N(C(C)=O)N=C(C)C1=O

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Application In Synthesis of [ 88513-00-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 88513-00-2 ]

[ 88513-00-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 932-53-6 ]
  • [ 108-24-7 ]
  • [ 88513-00-2 ]
YieldReaction ConditionsOperation in experiment
for 2h;Heating / reflux; <strong>[932-53-6]6-azathymine</strong> (commercially available from Alfa Aesar, 300 mg, 2.360 mmol), was suspended in acetyc anhydride (1.34 ml_, 14.20 mmol) and the mixture was refluxed for 2hours.The reaction mixture was then cooled to room temperature and dried under vacuum. The crude product was repeatedly treated with toluene and concentrated under reduced pressure to afford the title compound 2-acetyl-6-methyl-1 ,2,4-triazine-3,5(2H,4H)-dione that was used for next step without purification.MS (ES) (mlz): 170.06 [M+ H]+.
 

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