Alternatived Products of [ 89047-06-3 ]
Product Details of [ 89047-06-3 ]
CAS No. : | 89047-06-3 |
MDL No. : | MFCD28149707 |
Formula : |
C9H6ClNO
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
179.60
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 89047-06-3 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 89047-06-3 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 89047-06-3 ]
- 1
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[ 89047-03-0 ]
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[ 89047-06-3 ]
Yield | Reaction Conditions | Operation in experiment |
66% |
In toluene at 110℃; for 0.75h; |
|
- 2
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[ 112853-61-9 ]
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[ 89047-06-3 ]
Yield | Reaction Conditions | Operation in experiment |
91% |
With sodium methylate In methanol Heating; |
|
- 3
-
[ 35167-28-3 ]
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[ 13820-15-0 ]
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[ 89047-06-3 ]
Yield | Reaction Conditions | Operation in experiment |
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Stage #1: vinyl phenyl selenide; 3-chlorobenzonitrile oxide With triethylamine In chloroform at 20℃; for 12h;
Stage #2: With dihydrogen peroxide In chloroform at 20℃; for 0.333333h; |
|
- 4
-
polystyrene-supported vinyl selenide
[ No CAS ]
-
[ 34158-71-9 ]
-
[ 89047-06-3 ]
Yield | Reaction Conditions | Operation in experiment |
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Stage #1: 3-chlorobenzaldehyde oxime With N-chloro-succinimide In chloroform at 20℃; for 0.333333h;
Stage #2: polystyrene-supported vinyl selenide With triethylamine In dichloromethane at 20℃; for 12h;
Stage #3: With dihydrogen peroxide In tetrahydrofuran at 20℃; for 0.5h; Further stages.; |
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- 5
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[ 34158-71-9 ]
-
[ 89047-06-3 ]
Yield | Reaction Conditions | Operation in experiment |
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Multi-step reaction with 2 steps
1.1: N-chlorosuccinimide / CHCl3 / 0.33 h / 20 °C
2.1: Et3N / CHCl3 / 12 h / 20 °C
2.2: aq. H2O2 / CHCl3 / 0.33 h / 20 °C |
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- 6
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[ 33341-68-3 ]
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[ 89047-06-3 ]
Yield | Reaction Conditions | Operation in experiment |
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Multi-step reaction with 3 steps
1: triethylamine / diethyl ether / 0.17 h / -5 °C
2: diethyl ether / 12 h / Ambient temperature
3: 66 percent / toluene / 0.75 h / 110 °C |
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- 7
-
[ 13820-15-0 ]
-
[ 89047-06-3 ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 2 steps
1: diethyl ether / 12 h / Ambient temperature
2: 66 percent / toluene / 0.75 h / 110 °C |
|
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Multi-step reaction with 2 steps
1: 91 percent / n-butyllithium / tetrahydrofuran
2: 91 percent / sodium methoxide / methanol / Heating |
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Reference:
[1]Baranski, Andrzej; Shvekhgeimer, Genrikh A.
[Polish Journal of Chemistry, 1982, vol. 56, # 3, p. 459 - 467]
[2]Di Nunno, L.; Scilimati, A.
[Tetrahedron, 1987, vol. 43, # 9, p. 2181 - 2190]
- 8
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3-chlorobenzohydroximinoyl chloride
[ No CAS ]
-
[ 89047-06-3 ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 3 steps
1: benzene
2: 91 percent / n-butyllithium / tetrahydrofuran
3: 91 percent / sodium methoxide / methanol / Heating |
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