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Chemical Structure| 891270-49-8 Chemical Structure| 891270-49-8

Structure of 891270-49-8

Chemical Structure| 891270-49-8

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Product Details of [ 891270-49-8 ]

CAS No. :891270-49-8
Formula : C10H19IO2
M.W : 298.16
SMILES Code : ICCCCCC1(CC)OCCO1
MDL No. :MFCD25968459
InChI Key :NHYFABFQVIZNEB-UHFFFAOYSA-N
Pubchem ID :67269137

Safety of [ 891270-49-8 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H227-H301
Precautionary Statements:P210-P264-P270-P280-P301+P310+P330-P370+P378-P403+P235-P405-P501
Class:6.1
UN#:2810
Packing Group:

Application In Synthesis of [ 891270-49-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 891270-49-8 ]

[ 891270-49-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 891270-49-8 ]
  • [ 42726-73-8 ]
  • [ 942483-55-8 ]
YieldReaction ConditionsOperation in experiment
EXAMPLE 1 2-r5-(2-Naphthvn-lJg-imdazol-2-yll-8-oxodecanoic acid (A4) Step 1: fert-Butyl methyl r5-(2-ethyl-l,3-dioxolan-2-yl)pentyl1malonate (Al) To a suspension of NaH (60percent, 1 eq) in THF (0.1 M solution) at 0 0C was added dropwise tert- butyl methyl malonate (1 eq.) and the resulting mixture was stirred for 1 hr at RT and then added to a solution of 2-ethyl-2-(5-iodopentyl)-l,3-dioxolane (0.9 eq) in THF (0.3 M solution). The resulting mixture was stirred at 60 0C for 1 hr and then NH4Cl solution was added and the organic layer separated, dried (Na2SO4) and concentrated under reduced pressure to yield a colorless oil which was used without any further purification. 1H NMR (400 MHz, CDCl3) delta: 3.81 (4H, s), 3.61 (3H, s), 3.12 (IH, t, J = 7.4 Hz ), 1.80-1.67 (2H, m), 1.56-1.43 (4H, m), 1.34 (9H, s), 1.29-1.17 (6H, m), 0.79 (3H, t, J = 7.5 Hz). MS (ES) Ci8H32O6 requires: 344, found: 367 (M+Na)+.
 

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