Alternatived Products of [ 89438-55-1 ]
Product Details of [ 89438-55-1 ]
CAS No. : | 89438-55-1 |
MDL No. : | MFCD13192283 |
Formula : |
C11H14N2O
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | OXPAKOUDBFTPRL-UHFFFAOYSA-N |
M.W : |
190.24
|
Pubchem ID : | 163570 |
Synonyms : |
|
Application In Synthesis of [ 89438-55-1 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 89438-55-1 ]
- 1
-
[ 612-25-9 ]
-
[ 109-73-9 ]
-
[ 89438-55-1 ]
Yield | Reaction Conditions | Operation in experiment |
79% |
With carbon dioxide; In tetrahydrofuran; at 25℃; for 24h;UV-irradiation; |
Add 0.2 mmol I (where R1 = H) to a 10 mL reaction flask, 0.24mmol II (where R2=nC3H7) and 4mL THF, the atmosphere is carbon dioxide atmosphere, the light was irradiated by ultraviolet light at 25 C for 24 h. After the reaction was completed, it was filtered and concentrated. Chromatographically isolated III (where R1 = H; R2 = nC3H7), yield 79%. |
Reference:
[1]RSC Advances,2019,vol. 9,p. 13249 - 13253
[2]Patent: CN109734666,2019,A .Location in patent: Paragraph 0059-0060
[3]Organic Letters,2018,vol. 20,p. 4736 - 4739
[4]Chemistry - An Asian Journal,2019,vol. 14,p. 1436 - 1442
[5]Organic Letters,2019,vol. 21,p. 6058 - 6062
[6]Journal of Organic Chemistry,2018,vol. 83,p. 15493 - 15498