Home Cart Sign in  
Chemical Structure| 89789-67-3 Chemical Structure| 89789-67-3

Structure of 89789-67-3

Chemical Structure| 89789-67-3

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 89789-67-3 ]

CAS No. :89789-67-3
Formula : C5H16Cl2N2
M.W : 175.10
SMILES Code : CC(N)CCCN.[H]Cl.[H]Cl
MDL No. :MFCD28505983

Safety of [ 89789-67-3 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Application In Synthesis of [ 89789-67-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 89789-67-3 ]

[ 89789-67-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 349-02-0 ]
  • [ 89789-67-3 ]
  • 4,4-(pentane-1,4-diylbis(azanediyl))bis(3-nitrobenzamide) [ No CAS ]
YieldReaction ConditionsOperation in experiment
100% With N-ethyl-N,N-diisopropylamine; In isopropyl alcohol; at 105℃; for 18h;Sealed tube; Into a reaction flask was placed pentane-1,4-diamine, 2 hydrochloride (1 g, 5.71 mmol) and isopropanol (9.52 mL). To this solution was added <strong>[349-02-0]4-fluoro-3-nitrobenzamide</strong> (1.052 g, 5.71 mmol) followed by DIPEA (4.49 mL, 25.7 mmol). The flask was capped and the reaction was heated to 105 C. After 4 hours, more <strong>[349-02-0]4-fluoro-3-nitrobenzamide</strong> (1.052 g, 5.71 mmol) and isopropanol (10 mL) were added. The mixture was stirred overnight (~ 14 h) at 105 C. The formed precipitate was filtered off and rinsed with isopropanol twice (5 mL each). 4,4'-(Pentane-1,4-diylbis(azanediyl))bis(3-nitrobenzamide) (2.6 g, 5.80 mmol, 100% yield) was obtained as a yellow solid. LCMS (m/z): 431.3 [M + H]+
 

Historical Records