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[ CAS No. 897958-99-5 ] {[proInfo.proName]}

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Chemical Structure| 897958-99-5
Chemical Structure| 897958-99-5
Structure of 897958-99-5 * Storage: {[proInfo.prStorage]}
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Product Details of [ 897958-99-5 ]

CAS No. :897958-99-5 MDL No. :MFCD13177816
Formula : C8H6INO Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 259.04 Pubchem ID :-
Synonyms :

Safety of [ 897958-99-5 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 897958-99-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 897958-99-5 ]

[ 897958-99-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 103440-53-5 ]
  • [ 897958-99-5 ]
  • 2
  • [ 162607-17-2 ]
  • [ 897958-99-5 ]
  • [ 1567836-84-3 ]
YieldReaction ConditionsOperation in experiment
60% With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In ethanol; toluene;Reflux; Inert atmosphere; General procedure: Reaction of thiophene-2-boronic acid and 5-iodoisoindolin- 1-one according to general procedure C gave a crude product which was purified by flash column chromatography on silica gel (5% MeOH/CH2C12 as eluant) to give the title compound as a beige solid (60%), m.p. (CH2C12) 25 1-253C. ?H NMR[400 MHz, (CD3)2S0] 6 8.55 (br s, I H), 7.82 (br s, 1 H), 7.73 (dd, J = 7.9, 1.5 Hz, I H),7.68 (d, J 7.9 Hz, 1 H), 7.49 (d, J 3.9 Hz, I H), 7.31 (d, J 3.9 Hz, I H), 4.41 (s, 2 H).LRMS (APCI1) calcd for C,2H9BrNOS 294, 296 (MW), found 294, 296.Anal. (C12H8BrNOS) C, H, N.
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