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Chemical Structure| 90870-20-5 Chemical Structure| 90870-20-5

Structure of 90870-20-5

Chemical Structure| 90870-20-5

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Product Details of [ 90870-20-5 ]

CAS No. :90870-20-5
Formula : C10H12N2O4
M.W : 224.21
SMILES Code : O=C(OC1=CC=C([N+]([O-])=O)C=C1)N(CC)C

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Application In Synthesis of [ 90870-20-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 90870-20-5 ]

[ 90870-20-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 90870-20-5 ]
  • [ 105601-04-5 ]
  • [ 105601-20-5 ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate; In dimethyl sulfoxide; at 90 - 110℃; for 35 - 40h; 3- (1-dimethylaminoethyl) phenol (200gm, 1.21 moles), anhydrous potassium carbonate (252gm, 1.515 moles), N-ethyl-N-methyl-4-nitrophenyl carbamate (340gm, 1.82 moles) and dimethylsulfoxide [(1] liter) are mixed and heated at a temperature of about [90] to about [110C,] under nitrogen atmosphere, for 35-40 hours. The reaction mixture is cooled gradually to room temperature and filtered. The filtered solution is quenched in ice-water mixture and extracted with ethyl acetate to furnish racemic Rivastigmine.
 

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