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CAS No. : | 91062-38-3 | MDL No. : | MFCD06659852 |
Formula : | C10H13BO4 | Boiling Point : | 366.42°C at 760 mmHg |
Linear Structure Formula : | - | InChI Key : | N/A |
M.W : | 208.02 g/mol | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H317-H319 | Packing Group: | N/A |
GHS Pictogram: |
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Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With hydrogenchloride |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
p-Carboxy-phenylborsaeure, Propanol <90grad, 1h, in Ggw. v. HCl>; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With bis(triphenylphosphine)palladium(II) chloride; caesium carbonate In water; N,N-dimethyl-formamide at 80℃; for 18h; | 2. General procedure for the synthesis of 9. General procedure: To a DMF (35.0 mL/1 mmol of substrate) solution of a 7d-II or 7a or 7b (1 equiv) was added to bis(triphenylphosphine)palladium dichloride (0.2 equiv), cesium carbonate (2 equiv) and boronic acids 8 (2 equiv) in water (9.0 mL/1 mmol of substrate) at 80 °C. After being stirred at 80 °C for 18 h, the reaction mixture was quenched by addition of water and the product was extracted with ether three times. The combined organic extracts were washed with brine, dried over anhydrous magnesium sulfate, filtered, and concentrated under reduced pressure. The residue was purified by preparative TLC to give the title compound. |
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