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[ CAS No. 91062-38-3 ]

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Chemical Structure| 91062-38-3
Chemical Structure| 91062-38-3
Structure of 91062-38-3 * Storage: {[proInfo.prStorage]}

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Alternatived Products of [ 91062-38-3 ]

Product Details of [ 91062-38-3 ]

CAS No. :91062-38-3 MDL No. :MFCD06659852
Formula : C10H13BO4 Boiling Point : 366.42°C at 760 mmHg
Linear Structure Formula :- InChI Key :N/A
M.W :208.02 g/mol Pubchem ID :-
Synonyms :

Safety of [ 91062-38-3 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P280-P305+P351+P338 UN#:N/A
Hazard Statements:H317-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 91062-38-3 ]

  • Downstream synthetic route of [ 91062-38-3 ]

[ 91062-38-3 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 71-23-8 ]
  • [ 14047-29-1 ]
  • [ 91062-38-3 ]
YieldReaction ConditionsOperation in experiment
With hydrogenchloride
YieldReaction ConditionsOperation in experiment
p-Carboxy-phenylborsaeure, Propanol <90grad, 1h, in Ggw. v. HCl>;
  • 3
  • [ 1443293-87-5 ]
  • [ 91062-38-3 ]
  • (±)-2-{4-(4-propoxycarbonyl)phenyl}-1,4-dioxaspiro[4.5]deca-6,9-dien-8-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
With bis(triphenylphosphine)palladium(II) chloride; caesium carbonate In water; N,N-dimethyl-formamide at 80℃; for 18h; 2. General procedure for the synthesis of 9. General procedure: To a DMF (35.0 mL/1 mmol of substrate) solution of a 7d-II or 7a or 7b (1 equiv) was added to bis(triphenylphosphine)palladium dichloride (0.2 equiv), cesium carbonate (2 equiv) and boronic acids 8 (2 equiv) in water (9.0 mL/1 mmol of substrate) at 80 °C. After being stirred at 80 °C for 18 h, the reaction mixture was quenched by addition of water and the product was extracted with ether three times. The combined organic extracts were washed with brine, dried over anhydrous magnesium sulfate, filtered, and concentrated under reduced pressure. The residue was purified by preparative TLC to give the title compound.
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