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Chemical Structure| 915088-14-1 Chemical Structure| 915088-14-1

Structure of 915088-14-1

Chemical Structure| 915088-14-1

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Product Details of [ 915088-14-1 ]

CAS No. :915088-14-1
Formula : C24H26BNO2
M.W : 371.28
SMILES Code : CC1(C)C(C)(C)OB(C2=CC(N(C3=CC=CC=C3)C4=CC=CC=C4)=CC=C2)O1
InChI Key :QCXZGMTXGKIZBZ-UHFFFAOYSA-N
Pubchem ID :59207617

Safety of [ 915088-14-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 915088-14-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 915088-14-1 ]

[ 915088-14-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 915088-14-1 ]
  • [ 57103-20-5 ]
  • C36H25BrN2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
58% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In water; toluene;Inert atmosphere; Reflux; A mixture of 10 g of <strong>[57103-20-5]3,6-dibromo-9-phenyl-9H-carbazole</strong>,4.6 g of the intermediate 1 obtained in Preparation Example 1,0.3 g of Pd (PPh3) 4 and5.1 g of K2CO3 was placed in a round bottom three-necked flask under a nitrogen atmosphere,And 100 ml of toluene was added.The mixture was stirred and refluxed.After completion of the reaction, the resulting solution was washed with dichloromethane and water. Collecting organic layer,Dried over MgSO4 and separated by column,Thus, 4.1 g of intermediate 13 was obtained (yield 58percent).
  • 2
  • [ 915088-14-1 ]
  • [ 57103-20-5 ]
  • C54H39N3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
49% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In water; toluene;Inert atmosphere; Reflux; 2 g of <strong>[57103-20-5]3,6-dibromo-9-phenyl-9H-carbazole</strong>,3.9 g of the intermediate 1 synthesized in Preparation Example 1,0.3 g of Pd (PPh3) 4 and 4.1 g of K2CO3 were placed in a round bottom three-necked flask under a nitrogen atmosphere,And 50 ml of toluene was added.The mixture was stirred and refluxed.After completion of the reaction,The reaction solution was washed with dichloromethane and water.The moisture of the collected organic layer was then removed using MgSO4.The reaction mixture was separated by column and recrystallized,Thus, 1.8 g of compound 1 (yield 49percent) was obtained.
 

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