Home Cart Sign in  
Chemical Structure| 916435-41-1 Chemical Structure| 916435-41-1

Structure of 916435-41-1

Chemical Structure| 916435-41-1

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 916435-41-1 ]

CAS No. :916435-41-1
Formula : C12H6BrIO
M.W : 372.98
SMILES Code : IC1=CC=C(OC2=CC=C(Br)C=C23)C3=C1
MDL No. :MFCD28975101
InChI Key :YMEVNDQRPHHDRH-UHFFFAOYSA-N
Pubchem ID :67335932

Safety of [ 916435-41-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H319-H413
Precautionary Statements:P501-P273-P270-P264-P280-P337+P313-P305+P351+P338-P301+P312+P330

Application In Synthesis of [ 916435-41-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 916435-41-1 ]

[ 916435-41-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 5408-56-0 ]
  • [ 916435-41-1 ]
YieldReaction ConditionsOperation in experiment
62.2% With bromine; acetic acid; at 50 - 66℃; for 16h; 10 g (0.034 mol) of Exemplified Compound 3-1 and 200 ml of acetic acid were mixed, and 10.9 g (× 2 mol) of bromine was added dropwise in the vicinity of 50 C. over 10 minutes,And the mixture was further stirred for 16 hours. (Internal temperature 65 to 66 C.) After stirring at room temperature for 1 hour, filtration under reduced pressure was carried out.The obtained crystals were added to a THF / methanol mixture and the suspension was refluxed for 30 minutes. After stirring at room temperature for 1 hour, filtration under reduced pressure gave Exemplified Compound 2-1, 7.9 g. (Yield 62.2%) Identification of each compound in the examples was carried out by MASS and NMR spectra, and it was confirmed that they were the target compound. Exemplary compounds according to other general formulas [2] and [5] can also be synthesized according to the above-mentioned method.
 

Historical Records

Technical Information

Categories