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Chemical Structure| 917910-75-9 Chemical Structure| 917910-75-9

Structure of 917910-75-9

Chemical Structure| 917910-75-9

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Product Details of [ 917910-75-9 ]

CAS No. :917910-75-9
Formula : C14H12N2O2
M.W : 240.26
SMILES Code : COC1=CC=C(COC2=CN=C(C=C2)C#N)C=C1
MDL No. :MFCD18452162

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Application In Synthesis of [ 917910-75-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 917910-75-9 ]

[ 917910-75-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 327056-62-2 ]
  • [ 105-13-5 ]
  • [ 917910-75-9 ]
YieldReaction ConditionsOperation in experiment
50% With potassium carbonate; In N,N-dimethyl-formamide; at 105℃; for 16h; 5-Fluoropyridine-2-carbonitrile 61a (2.68 g, 21.9 mmol), 4-methoxybenzyl alcohol (2.76 g, 20.0 mmol) andPotassium carbonate (3.31 g, 23.7 mmol) was added to N,N-dimethylformamide (10 mL), and the reaction was stirred at 105 C for 16 hours.Ethyl acetate/petroleum ether (v/v = 5/1, 25 mL) was added to the reaction mixture, and a large white solid was precipitated and filtered.The filter cake is dried to obtain the title compound61b (2.4 g, yield 50%) as a white solid.
 

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